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[ CAS No. 882518-89-0 ] {[proInfo.proName]}

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Chemical Structure| 882518-89-0
Chemical Structure| 882518-89-0
Structure of 882518-89-0 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 882518-89-0 ]

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Product Details of [ 882518-89-0 ]

CAS No. :882518-89-0 MDL No. :MFCD27977515
Formula : C17H26O7S Boiling Point : No data available
Linear Structure Formula :- InChI Key :NIPMXQFRYHXBAM-UHFFFAOYSA-N
M.W : 374.45 Pubchem ID :59766026
Synonyms :
Chemical Name :tert-Butyl 2-(2-(2-(tosyloxy)ethoxy)ethoxy)acetate

Safety of [ 882518-89-0 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 882518-89-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 882518-89-0 ]

[ 882518-89-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 5292-43-3 ]
  • [ 118591-58-5 ]
  • [ 882518-89-0 ]
YieldReaction ConditionsOperation in experiment
83.9% With tetrabutylammomium bromide; potassium hydroxide; In toluene; at 20℃; Compound 2a (2.954 g, 11.3 mmol) was dissolved in 10 mL of toluene, TBAB (0.181 g, 0.56 mmol), KOH (1.01 g, 18.1 mmol), tert-butyl bromoacetate (2.7 g, 13.6 mmol) . The reaction was stirred at room temperature overnight. After thin layer chromatography (PE: EA = 1:2), the raw material remained. Toluene was concentrated under reduced pressure, and 5 mL of water was added, and the mixture was extracted three times with 15 mL of dichloromethane. Column chromatography (EA) gave 3.4 g of product, yield 83.9%.
83.9% With tetrabutylammomium bromide; potassium hydroxide; In toluene; at 20℃; Compound 2a (2.954 g, 11.3 mmol) was dissolved in 10 mL of toluene, TBAB (0.181 g, 0.56 mmol), KOH (1.01 g, 18.1 mmol), tert-butyl bromoacetate (2.7 g, 13.6 mmol) .The reaction was stirred at room temperature overnight.After thin layer chromatography (PE: EA = 1:2), the raw material remained.The toluene was concentrated under reduced pressure, and 5 mL of water was added, and the mixture was extracted three times with 15 mL of dichloromethane.Column chromatography (EA) gave 3.4 g of product, yield 83.9percent.
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