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CAS No. : | 853-67-8 | MDL No. : | MFCD00053255 |
Formula : | C14H6Na2O8S2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | CSCLXYAAXMCWLG-UHFFFAOYSA-L |
M.W : | 412.30 | Pubchem ID : | 70069 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With trichlorophosphate; In sulfolane; acetonitrile; for 20.0h;Heating / reflux; | EXAMPLE 10A 9,10-dioxo-9,10-dihydro-2,7-anthracenedisulfonyl dichloride Anthraquinone-2,7-disulfonic acid disodium salt (1.24 g, 3 mmol) and sulfolane (5 ml) in acetonitrile (5 ml) was treated with phosphorous oxychloride (2.3 ml, 25 mmol). The mixture was heated at reflux for 20 hours, allowed to cool to room temperature, and filtered through a pad of silica gel with methylene chloride. The filtrate was concentrated under reduced pressure and the crude product was used in the next step without further purification. |
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