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[ CAS No. 78-26-2 ] {[proInfo.proName]}

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Chemical Structure| 78-26-2
Chemical Structure| 78-26-2
Structure of 78-26-2 * Storage: {[proInfo.prStorage]}

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Product Details of [ 78-26-2 ]

CAS No. :78-26-2 MDL No. :MFCD00004696
Formula : C7H16O2 Boiling Point : -
Linear Structure Formula :HOCH2C(CH3)(C3H7)CH2OH InChI Key :JVZZUPJFERSVRN-UHFFFAOYSA-N
M.W : 132.20 Pubchem ID :66220
Synonyms :
Chemical Name :2-Methyl-2-propylpropane-1,3-diol

Safety of [ 78-26-2 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H332-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 78-26-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 78-26-2 ]

[ 78-26-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 51792-34-8 ]
  • [ 78-26-2 ]
  • 3-methyl-3-propyl-3,4-dihydro-2H-thieno[3,4-b][1,4]dioxepine [ No CAS ]
YieldReaction ConditionsOperation in experiment
80% With toluene-4-sulfonic acid; In toluene; at 110℃; for 24h; As shown in Scheme 5 below, to 100 mL of toluene in which 5.28 g (27.7 mmol) of p-toluenesulfonic acid (p-TSA ), 20.0 g (138.7 mmol) of <strong>[51792-34-8]3,4-dimethoxythiophene</strong> (compound (1)) and 2-methyl-2-Propyl-1,3-propanediol, compound (8)) were mixed and stirred at 110 DEG C for 24 hours. After completion of the reaction, a mixed solvent of water and ethyl acetate (EtOAc) was added to the reaction product, extracted, washed with brine, water removed using anhydrous Na2SO4, filtered and concentrated. The water was separated by column chromatography on SiO2 (eluent: hexane: ethyl acetate = 10: 1) to give 3-methyl-3-propyl-3,4-dihydro-2H-thieno [3,4-b] [1,4] dioxepin -B] [1,4] dioxepine, compound (9)) (yield: 65-80percent). Of the obtained compound 1H-NMR the data is as follows : 1H-NMR (CDCl3, Varian 400 MHz) : delta 0.93-0.96 (6H, m), 1.29-1.45 (4H, m), 3.69-3.88 (4H,m), 6.45 (2H, s).
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