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[ CAS No. 73789-86-3 ] {[proInfo.proName]}

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Type HazMat fee for 500 gram (Estimated)
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Limited Quantity USD 15-60
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Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
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Chemical Structure| 73789-86-3
Chemical Structure| 73789-86-3
Structure of 73789-86-3 * Storage: {[proInfo.prStorage]}

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Product Details of [ 73789-86-3 ]

CAS No. :73789-86-3 MDL No. :MFCD03427264
Formula : C10H13Br Boiling Point : No data available
Linear Structure Formula :(CH(CH3)2)C6H4CH2Br InChI Key :YXTHBZLABLYGEE-UHFFFAOYSA-N
M.W : 213.11 Pubchem ID :47719
Synonyms :

Safety of [ 73789-86-3 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:1760
Hazard Statements:H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 73789-86-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 73789-86-3 ]

[ 73789-86-3 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 150008-24-5 ]
  • [ 73789-86-3 ]
  • C20H30N2O3 [ No CAS ]
  • 2
  • [ 73789-86-3 ]
  • [ 189680-06-6 ]
  • C17H16BrNO [ No CAS ]
YieldReaction ConditionsOperation in experiment
100% With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 20℃; for 18.0h; a- Synthesis of Int. 88: A sol. of <strong>[189680-06-6]2-bromo-5-hydroxybenzonitrile</strong> (6.29 g, 31.8 mmol) in ACN (90 mL) and DMF (10 mL) was treated with K2C03 (4.83 g, 34.9 mmol) and 8 (7.11 g, 33.4 mmol) at rt. The r.m. was stirred for 18 h at r.t. Then, water and EtOAc were added, and the organic layer was washed with brine, separated, dried over MgS04, filtered and concentrated in vacuo to afford 11.4 of Int. 88, white solid (quant.).
100% With potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; at 20℃; for 18.0h; a- Synthesis of intermediate 13: A solution of <strong>[189680-06-6]2-bromo-5-hydroxybenzonitrile</strong> (6.29 g, 31.8 mmol) in ACN (90 mL) and DMF (10 mL) was treated with K2C03 (4.83 g, 34.9 mmol) and 4-isopropylbenzyl bromide (7.11 g, 33.4 mmol) at r.t. The reaction mixture was stirred for 18 hours at r.t. Then, water and EtOAc were added, and the organic layer was washed with brine,separated, dried over MgSO4, filtered and concentrated in vacuo to afford 11.4 g of intermediate 13, white solid (quantitative).
  • 3
  • [ 1196156-42-9 ]
  • [ 73789-86-3 ]
  • C18H19N3O2 [ No CAS ]
  • methyl 1-(4-isopropylbenzyl)-1H-pyrazolo[3,4-b]pyridine-5-carboxylate [ No CAS ]
  • 4
  • [ 89942-77-8 ]
  • [ 73789-86-3 ]
  • C18H19NO5 [ No CAS ]
YieldReaction ConditionsOperation in experiment
General procedure: Compound 1 (10 mmol), anhydrous potassium carbonate (20 mmol, K2CO3) and DMF (20 mL) were added to a 100 mL-dry eggplant flask and stirred at room temperature for 30 min prior to addition of p-bromobenzyl bromide (12 mmol). The resulting mixture was maintained at 80 C for 3-8 h, and the reaction course was monitored using TLC. Upon the reaction completion, the mixture was cooled to room temperature before the addition of 100mL of water, and the system was extracted with ethyl acetate (30 mL 3). The organic phase was dried over anhydrous Na2SO4 and concentrated using rotary evaporator. The crude product 2 was used in the next step without further purification.
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