[ CAS No. 73568-26-0 ] {[proInfo.proName]}

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2D 3D

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Quality Control of [ 73568-26-0 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 73568-26-0 ]

SDS Specification

Alternatived Products of [ 73568-26-0 ]

Product Details of [ 73568-26-0 ]

CAS No. :	73568-26-0	MDL No. :	MFCD02227041
Formula :	C₁₁H₈ClNO	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	YPBRSXNRWFUUOE-UHFFFAOYSA-N
M.W :	205.64	Pubchem ID :	689082
Synonyms :

Safety of [ 73568-26-0 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P305+P351+P338	UN#:	N/A
Hazard Statements:	H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 73568-26-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 73568-26-0 ]

[ 73568-26-0 ] Synthesis Path-Downstream 1~3

1
[ 73568-26-0 ]
[ 145214-05-7 ]
[ 1167542-08-6 ]

Yield	Reaction Conditions	Operation in experiment
34%	tetrakis(triphenylphosphine) palladium(0); In 1,2-dimethoxyethane; at 100℃; for 2.75h;microwave irradiation;	To a solution of 2-chloro-8-methylquinoline-3-carboxaldehyde (250 mg, 1.21 mmol) in DME (3 mL) was added <strong>[145214-05-7]2-(tributylstannyl)oxazole</strong> (0.31 mL, 1.76 mmol) and Pd(PPh3 )4 (70 mg, 0.06 mmol). The reaction mixture was heated in a microwave at 1000C for 45 minutes. More Pd(PPh3)4 (50 mg, 0.04 mmol) was added to the mixture, which was heated at 1000C for 2 h. Purification by column chromatography (SiO2, 0- 100% EtOAc in heptane) gave the title compound as a cream solid (99 mg, 34%). 8R (DMSO-d6) 10.85 (s, IH), 8.91 (s, IH), 8.52 (d, J0.6 Hz, IH), 8.12 (d, J8.1 Hz, IH), 7.86 (d, J 7.0 Hz, IH), 7.64-7.72 (m, 2H), 2.81 (s, 3H). LCMS (ES+) 239 (M+H)+, RT 3.65 minutes (Method 3).

Reference： [1]Patent: WO2009/81105,2009,A2 .Location in patent: Page/Page column 35

2
[ 73568-26-0 ]
[ 136812-21-0 ]

Reference： [1]Green Chemistry,2018,vol. 20,p. 266 - 273
[2]Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2009,vol. 48,p. 152 - 154
[3]Tetrahedron,2011,vol. 67,p. 9219 - 9224

3
[ 784-04-3 ]
[ 73568-26-0 ]
C₂₇H₁₈ClNO [ No CAS ]

Reference： [1]Medicinal Chemistry,2015,vol. 11,p. 580 - 589

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Isomers

Technical Information

? Alkyl Halide Occurrence ? Barbier Coupling Reaction ? Baylis-Hillman Reaction ? Bucherer-Bergs Reaction ? Clemmensen Reduction ? Complex Metal Hydride Reductions ? Corey-Chaykovsky Reaction ? Corey-Fuchs Reaction ? Fischer Indole Synthesis ? General Reactivity ? Grignard Reaction ? Hantzsch Dihydropyridine Synthesis ? Henry Nitroaldol Reaction ? Hiyama Cross-Coupling Reaction ? Horner-Wadsworth-Emmons Reaction ? Hydride Reductions ? Julia-Kocienski Olefination ? Kinetics of Alkyl Halides ? Knoevenagel Condensation ? Kumada Cross-Coupling Reaction ? Leuckart-Wallach Reaction ? McMurry Coupling ? Meerwein-Ponndorf-Verley Reduction ? Mukaiyama Aldol Reaction ? Nozaki-Hiyama-Kishi Reaction ? Passerini Reaction ? Paternò-Büchi Reaction ? Petasis Reaction ? Pictet-Spengler Tetrahydroisoquinoline Synthesis ? Preparation of Aldehydes and Ketones ? Preparation of Amines ? Prins Reaction ? Reactions of Aldehydes and Ketones ? Reactions of Alkyl Halides with Reducing Metals ? Reactions of Amines ? Reformatsky Reaction ? Schlosser Modification of the Wittig Reaction ? Schmidt Reaction ? Stetter Reaction ? Stille Coupling ? Stobbe Condensation ? Substitution and Elimination Reactions of Alkyl Halides ? Suzuki Coupling ? Tebbe Olefination ? Ugi Reaction ? Wittig Reaction ? Wolff-Kishner Reduction

Historical Records

Related Functional Groups of
[ 73568-26-0 ]

Chlorides

[ 73568-31-7 ]

2-Chloro-6,8-dimethylquinoline-3-carbaldehyde

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[ 938138-94-4 ]

2,6-Dichloro-8-methylquinoline-3-carbaldehyde

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[ 73568-25-9 ]

2-Chloroquinoline-3-carbaldehyde

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[ 73568-27-1 ]

2-Chloro-6-methylquinoline-3-carbaldehyde

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[ 323196-71-0 ]

2-Chloro-5,8-dimethylquinoline-3-carbaldehyde

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Aldehydes

[ 73568-31-7 ]

2-Chloro-6,8-dimethylquinoline-3-carbaldehyde

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[ 938138-94-4 ]

2,6-Dichloro-8-methylquinoline-3-carbaldehyde

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[ 73568-25-9 ]

2-Chloroquinoline-3-carbaldehyde

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[ 73568-27-1 ]

2-Chloro-6-methylquinoline-3-carbaldehyde

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[ 323196-71-0 ]

2-Chloro-5,8-dimethylquinoline-3-carbaldehyde

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Related Parent Nucleus of
[ 73568-26-0 ]

Quinolines

[ 73568-31-7 ]

2-Chloro-6,8-dimethylquinoline-3-carbaldehyde

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[ 938138-94-4 ]

2,6-Dichloro-8-methylquinoline-3-carbaldehyde

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[ 73568-25-9 ]

2-Chloroquinoline-3-carbaldehyde

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[ 323196-71-0 ]

2-Chloro-5,8-dimethylquinoline-3-carbaldehyde

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P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
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P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
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P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
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P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
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P370 + P378	In case of fire:
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P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
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P401
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H200	Unstable explosive
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H401	Toxic to aquatic life
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H411	Toxic to aquatic life with long-lasting effects
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[ CAS No. 73568-26-0 ] {[proInfo.proName]}

Quality Control of [ 73568-26-0 ]

Related Doc. of [ 73568-26-0 ]

Product Details of [ 73568-26-0 ]

Safety of [ 73568-26-0 ]

Application In Synthesis of [ 73568-26-0 ]

[ 73568-26-0 ] Synthesis Path-Downstream 1~3

Technical Information

Related Functional Groups of [ 73568-26-0 ]

Chlorides

Aldehydes

Related Parent Nucleus of [ 73568-26-0 ]

Quinolines

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

Inquiry

Related Functional Groups of
[ 73568-26-0 ]

Related Parent Nucleus of
[ 73568-26-0 ]