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[ CAS No. 712-76-5 ] {[proInfo.proName]}

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Chemical Structure| 712-76-5
Chemical Structure| 712-76-5
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Product Details of [ 712-76-5 ]

CAS No. :712-76-5 MDL No. :MFCD01310838
Formula : C13H13N Boiling Point : -
Linear Structure Formula :C6H5C6H4CH2NH2 InChI Key :RMSPOVPGDBDYKH-UHFFFAOYSA-N
M.W : 183.25 Pubchem ID :344989
Synonyms :

Safety of [ 712-76-5 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 712-76-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 712-76-5 ]

[ 712-76-5 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 486437-06-3 ]
  • [ 712-76-5 ]
  • [ 68957-94-8 ]
  • [ 486434-73-5 ]
YieldReaction ConditionsOperation in experiment
With 4-methyl-morpholine; In dichloromethane; ethyl acetate; Example 11 N-(biphenyl-4-yl)methyl-4-(4'-trifluoromethylbiphenyl-2-carbonylamino)-1-methyl-imidazol-2-carboxylic acid amide A solution of 100 mg (0.25 mmol) of 4-(4'-trifluoromethyl-biphenyl-2-carbonylamino)-1-methyl-imidazol-2-carboxylic acid, 48 mg (0.25 mmol) of 4-phenylbenzylamine and 0.2 ml (1.5 mmol) of N-methylmorpholine in 6 ml of dichloromethane is combined with 0.3 ml (0.5 mmol) of propanephosphonic acid cycloanhydride (50 wt. % in ethyl acetate) at -10 C. and stirred for 2 hours with cooling. Then it is washed with 2 molar hydrochloric acid and 2 molar sodium hydroxide solution, the combined organic extracts are dried and concentrated by evaporation. Yield: 0.12 g (84% of theory), Rf value: 0.59 (silica gel; dichloromethane/ethanol=9:1)
  • 2
  • 3-(biphenyl-2-carbonylamino)-benzoic acid [ No CAS ]
  • [ 712-76-5 ]
  • [ 68957-94-8 ]
  • N-(biphenyl-4-methyl)-3-(biphenyl-2-carbonylamino)-benzoic acid amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
88% With 4-methyl-morpholine; In dichloromethane; EXAMPLE 28 N-(biphenyl-4-methyl)-3-(biphenyl-2-carbonylamino)-benzoic acid amide Prepared analogously to Example 7 from 3-(biphenyl-2-carbonyl-amino)-benzoic acid and 4-phenylbenzylamine in dichloromethane with the addition of propanephosphonic acid cycloanhydride and N-methylmorpholine. Yield:88% of theory Rf value:0.76 (silica gel; dichloromethane/ethanol=95:5)
  • 3
  • [ 1053977-18-6 ]
  • [ 712-76-5 ]
  • [ 68957-94-8 ]
  • N-(biphenyl-4-methyl)-4-methyl-3-(biphenyl-2-carbonylamino)-benzoic acid amide [ No CAS ]
YieldReaction ConditionsOperation in experiment
30% With 4-methyl-morpholine; In dichloromethane; EXAMPLE 55 N-(biphenyl-4-methyl)-4-methyl-3-(biphenyl-2-carbonylamino)-benzoic acid amide Prepared analogously to Example 7 from 3-(biphenyl-2-carbonylamino)-4-methyl-benzoic acid and biphenyl-4-methylamine in dichloromethane with the addition of propanephosphonic acid cycloanhydride and N-methylmorpholine. Yield:30% of theory Rf value:0.73 (silica gel; dichloromethane/ethanol=9:1)
  • 4
  • [ 712-76-5 ]
  • [ 51997-51-4 ]
  • 1-((9H-carbazol-4-yl)oxy)-3-(([1,1'-biphenyl]-4-ylmethyl)amino)propan-2-ol [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% In isopropyl alcohol; for 5h;Inert atmosphere; Reflux; General procedure: Corresponding 2-(aryloxymethyl)oxiranes (5 mmol, 1 equiv) and amines (7.5 mmol, 1.5 equiv) were dissolved in 30 mL i-PrOH. The reaction was purged with argon 3 times and stirred at reflux for 5 h, andthen the mixture was cooled to room temperature and added AcOEt.After washing with brine 3 times, the organic layer was dried overanhydrous Na2SO4, filtered, and evaporated in vacuo. Purification ofthe crude residue by column chromatography on silica gel yielded target compounds.
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