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CAS No. : | 6575-09-3 | MDL No. : | MFCD00001782 |
Formula : | C8H6ClN | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 151.59 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Danger | Class: | 6.1 |
Precautionary Statements: | P261-P280-P305+P351+P338-P310 | UN#: | 3439 |
Hazard Statements: | H302-H311-H315-H319-H332 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
1.5 g | With sulfuric acid; at 100℃; | A solution of 2-chloro-6-methylbenzonitrile (2.0 g) in cone, sulphuric acid (10 mL) was heated at 100C for 3-4 h. The reaction mass was quenched in ice-water and the solid obtained was filtered. The precipitate was suck dried to afford 1.5 g of desired product. 1H NMR (300 MHz, DMSO d6): delta 2.28 (s, 3H), 7.21- 7.27 (m, 3H), 7.65 (s, 1H), 7.91 (s, 1H). |
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