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[ CAS No. 65451-89-0 ] {[proInfo.proName]}

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Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
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Chemical Structure| 65451-89-0
Chemical Structure| 65451-89-0
Structure of 65451-89-0 * Storage: {[proInfo.prStorage]}

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Product Details of [ 65451-89-0 ]

CAS No. :65451-89-0 MDL No. :MFCD06761896
Formula : C10H15NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 181.23 Pubchem ID :-
Synonyms :

Safety of [ 65451-89-0 ]

Signal Word:Danger Class:8
Precautionary Statements:P264-P270-P280-P302+P352-P305+P351+P338-P310-P330-P332+P313-P362-P501 UN#:2735
Hazard Statements:H302-H315-H318 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 65451-89-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 65451-89-0 ]

[ 65451-89-0 ] Synthesis Path-Downstream   1~13

  • 1
  • [ 65451-89-0 ]
  • [ 390811-94-6 ]
  • 1-cyclohexyl-2-pyridin-2-yl-1<i>H</i>-benzoimidazole-5-carboxylic acid [1-(3,4-dimethoxy-phenyl)-ethyl]-amide [ No CAS ]
  • 2
  • [ 2032-35-1 ]
  • [ 65451-89-0 ]
  • (S)-(-)-N-(2,2-diethoxyethyl)-1-(3,4-dimethoxyphenyl)ethylamine [ No CAS ]
  • 3
  • [ 65451-89-0 ]
  • [ 493-48-1 ]
  • 4
  • [ 944256-03-5 ]
  • [ 65451-89-0 ]
YieldReaction ConditionsOperation in experiment
With 1,3-dimethylbarbituric acid;tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenylphosphine; In dichloromethane; for 3h;Heating / reflux; D. A 50-mL round bottom flask was charged with Compound 18d (0.40 g, 1.53 mmol) and dichloromethane (8.0 ml_). Pd2(dba)3- CHCI3 (0.16 g, 0.15 mmol), triphenylphosphine (0.16 g, 6.1 mmol), and 1 ,3-dimethylbarbituric acid (0.79 g, 5.06 mmol) were added and the mixture was heated to reflux for 3 h. The mixture was cooled to room temperature, transferred to a separatory funnel, and extracted with 1 N HCI (50 ml_). The aqueous layer was basified with 3N NaOH and extracted with ethyl acetate (200 ml_). The organic layer was dried with MgSO4 and filtered through Celite to give Compound 18e as a white solid. 1H NMR (300 MHz, CDCI3) δ 6.74-6.85 (m, 3 H), 3.96-4.08 (m, 1 H), 3.83 (m, 3 H), 3.80 (m, 3 H), 1.87-1.97 (bs, 2 H), and 1.31 (d, J = 6.6 Hz, 3 H).
  • 5
  • [ 1010385-16-6 ]
  • [ 65451-89-0 ]
  • 6
  • [ 79-22-1 ]
  • [ 65451-89-0 ]
  • [ 1010385-47-3 ]
  • 7
  • [ 37418-88-5 ]
  • [ 65451-89-0 ]
  • [ 1190089-38-3 ]
  • 8
  • [ 85-44-9 ]
  • [ 65451-89-0 ]
  • (S)-(2-(1-phenyl)ethyl)isoindolin-1,3-dione [ No CAS ]
YieldReaction ConditionsOperation in experiment
89% at 100 - 150℃;Green chemistry; General procedure: An amount of 327.43 mg (1.1 mmol) of phthalic anhydrideand 243.56 mg (1 mmol) of phenylethylamine were placedinto a 50-mL round-bottom flask. The mixture was stirredand heated to gentle boil 100-150 C for 5-10 min. Thereaction was cooled at room temperature and monitored byTLC. Then the appropriate solvent (40 mL) was added andthe reaction was sonicated until a white powder formed. Theprecipitate was filtered, dissolved in acetone and precipitatedagain with water (pH 13).
  • 9
  • [ 91-13-4 ]
  • [ 65451-89-0 ]
  • (S)-2-(1-phenyl)ethyl-1,3-dihydroisoindoline hydrobromide [ No CAS ]
YieldReaction ConditionsOperation in experiment
97% at 150℃;Green chemistry; General procedure: An amount of 433.80 mg (1.6435 mmol) of α,α′-dibromo-oxyleneand 199.16 mg (1.6435 mmol) phenylethylaminewere placed into a 50-mL round-bottom flask. The mixturewas stirred and heated to gentle boil 150-250 C for 5-10min. The reaction was cooled at room temperature andmonitored by TLC. Afterwards, ethyl acetate (40 mL) wasadded and the reaction was sonicated until a white powder(hydrobromide) formed. The precipitate was filtered andwashed twice with acetone.
  • 10
  • [ 50919-08-9 ]
  • isopropyl 2-propoxyacetate [ No CAS ]
  • (R)-2-propoxy-N-(1-(3,4-dimethoxyphenyl)ethyl)acetamide [ No CAS ]
  • [ 65451-89-0 ]
YieldReaction ConditionsOperation in experiment
24% With lipase B from Candida antarctica immobilized on acrylic beads; In toluene; at 30℃; for 8h;Resolution of racemate; Enzymatic reaction; General procedure: Into a screw cap reaction vial were added a mixture of dry toluene (1.0 mL), immobilized CaLB enzyme (15.0 mg, CaLB-CV-T2-150), the corresponding racemic amine rac-1a-d (0.778 mmol) and the corresponding isopropyl 2-alkoxyacetate 2A-D (1.0 equiv., 0.778 mmol). The reaction mixture was shaken (750 rpm) at 30 C and monitored by taking samples (20 mL) after different reaction times (0.25, 0.5, 1, 2, 3, 4, 6, 8 h). After 8 h, the reactions were worked up.
  • 11
  • [ 1337958-31-2 ]
  • [ 65451-89-0 ]
  • C22H36BrNO3Si [ No CAS ]
  • C22H36BrNO3Si [ No CAS ]
  • 12
  • [ 2568-36-7 ]
  • [ 65451-89-0 ]
  • C16H22BrNO2 [ No CAS ]
  • 13
  • 7-chlorobenzo[c][1,2,5]oxadiazole-4-sulfonic acid chloride [ No CAS ]
  • [ 65451-89-0 ]
  • (+)-(S)-7-chloro-N-(1-(3,4-dimethoxyphenyl)ethyl)benzo(c)(1,2,5)oxadiazole-4-sulfonamide [ No CAS ]
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