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CAS No. : | 65055-17-6 | MDL No. : | MFCD00236215 |
Formula : | C7H3Cl2FO | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | DLZUHSFUBZTBQZ-UHFFFAOYSA-N |
M.W : | 193.00 | Pubchem ID : | 2736548 |
Synonyms : |
|
Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P501-P234-P264-P280-P390-P303+P361+P353-P301+P330+P331-P363-P304+P340+P310-P305+P351+P338+P310-P406-P405 | UN#: | 3261 |
Hazard Statements: | H314-H290 | Packing Group: | Ⅱ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
97.29% | In methanol; at 60℃; for 1h; | Example 1 Preparation of methyl 3-chloro-4-fluoro-benzoate In a 250 ml four-necked round bottom flask, equipped with a mechanical stirrer, condenser and thermometer, 86.5 g of 3-chloro-4-fluoro-benzoic acid chloride are loaded and 28.1 g of anhydrous MeOH are added by a dosing funnel. The reaction is exothermic and spontaneously reaches 60C. The methanol is metered keeping the temperature at about 60. It is stirred for 1 hour then the excess methanol is distilled. In this way 80 g of yellow oil are obtained corresponding to the compound methyl 3-chloro-4-fluoro-benzoate. Yield 97.29%. |
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