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CAS No. : | 63875-01-4 | MDL No. : | MFCD06410683 |
Formula : | C7H7NO | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | SUMAWDZJEIQACJ-UHFFFAOYSA-N |
M.W : | 121.14 | Pubchem ID : | 2763000 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
20% | With pyridine; chromium(VI) oxide; In dichloromethane; at 20℃; for 0.5h; | A solution of chromium (Vl) oxide (2 g, 20 mmol), pyridine (4 mL, 50 mmol) and 20 mL of dichloromefhane was stirred at room temperature for 30 minutes. To this mixture, cooled with an ice water bath, (2-methyl-pyridin-4-yl)-methanol (48, 0.5 g, 4.0 mmol) in 5 mL of dichloromethane was added. The reaction mixture was stirred at room temperature for 30 minutes. The reaction mixture was cooled with an ice water bath and diluted with ethyl acetate, then filtered through a pad of Celite, The filtrate was concentrated under vacuum and the residue was purified by silica gel chromatography eluting with hexanes and ethyl acetate to provide the desired compound as a colorless liquid (21b, 0.1 g, 20%), |
With manganese(IV) oxide; In chloroform; for 18h;Heating / reflux; | Example 32: Preparation of 2-methyl-pyridine-4-carbaldehvde; [00421] (2-Methyl-pyridin-4-yl)-methanol (1.3 g, 10.6 mmol) (prepared according to the literature procedure, see Ragan, J.A. etal. Synthesis, 2002, 4, 483-486) and MnO2 (5 .0 g, 57.5 mmol) in CHCI3 (50 mL) was refluxed for 18 h. The reaction mixture was cooled to room temperature and filtered. The filter cake was washed with CHCI3 (2 x 100 mL). The combined filtrates were concentrated under reduced pressure and the resulting residue was purified by flash column chromatography on silica gel (EtOAc/Hexanes, 3:7) to provide desired aldehyde. Mass spectrum m/z : 122.1 (M+H). |
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