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[ CAS No. 627906-52-9 ] {[proInfo.proName]}

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Chemical Structure| 627906-52-9
Chemical Structure| 627906-52-9
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Product Details of [ 627906-52-9 ]

CAS No. :627906-52-9 MDL No. :MFCD16994279
Formula : C13H19BO3 Boiling Point : No data available
Linear Structure Formula :- InChI Key :WWKXCYNPIQEAKJ-UHFFFAOYSA-N
M.W : 234.10 Pubchem ID :51358338
Synonyms :

Safety of [ 627906-52-9 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 627906-52-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 627906-52-9 ]

[ 627906-52-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 68500-37-8 ]
  • [ 627906-52-9 ]
  • HY-112667 [ No CAS ]
YieldReaction ConditionsOperation in experiment
85% With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium carbonate; In 1,4-dioxane; water; at 100℃;Inert atmosphere; (0574) A mixture of 4-chloro-7-methoxy-quinolone (80 mg, 0.42 mmol), 2-methyl- 4-(4,4,5,5-tetramethyl- 1,3,2-dioxaborolan-2-yl)phenol (97 mg, 0.42 mmol), K2C03 (158mg, l. lmmol) and [1,1'- bis(diphenylphosphino)ferrocene]dichloropalladium (II), complex with dichloromethane (18 mg, 0.01 mmol) in dioxane (5 mL) and H20 (1 mL) was heated at 100 C overnight in an atmosphere of nitrogen. The reaction was then quenched with water and extracted with ethyl acetate. The combined organic layers were dried over magnesium sulfate, filtered and concentrated. The residue was purified by flash column chromatography on silica gel (eluent: (0575) dichloromethane/methanol, 0-10%) to give the title compound as white solid (77 mg, 85%). ESI-MS m/z: 266.1181[M+H]+; Purity: 99.0%. 1H NMR (400 MHz, DMSO-c 6) delta 9.69 (s, 1H), 8.79 (d, J = 4.5 Hz, 1H), 7.85 (d, J = 9.3 Hz, 1H), 7.44 (d, J = 2.6 Hz, 1H), 7.26 - 7.20 (m, 3H), 7.20 - (0576) 7.16 (m, 1H), 6.95 (d, J= 8.2 Hz, 1H), 3.93 (s, 3H), 2.21 (s, 3H); 13C NMR (101 MHz, DMSO) delta 159.84, 155.98, 150.27, 150.14, 147.57, 131.66, 127.96, 127.90, 126.93, 124.32, 121.13, 119.20, 119.12, 114.71, 107.77, 55.46, 16.03.
  • 2
  • [ 68500-37-8 ]
  • [ 627906-52-9 ]
  • C16H13NO2 [ No CAS ]
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