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CAS No. : | 620-19-9 | MDL No. : | MFCD00000909 |
Formula : | C8H9Cl | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | LZBOHNCMCCSTJX-UHFFFAOYSA-N |
M.W : | 140.61 | Pubchem ID : | 12102 |
Synonyms : |
|
Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P261-P280-P305+P351+P338-P310 | UN#: | 3265 |
Hazard Statements: | H314-H335 | Packing Group: | Ⅱ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
78% | With sulfur; potassium hydroxide; In dimethyl sulfoxide; at 130℃; for 24h;Sealed tube; | General procedure: A mixture of benzamidine hydrochloride (0.5 mmol), benzyl chloride (0.5 mmol), sulfur powder (0.375 mmol), KOH (1.5 mmol) and dimethyl sulfoxide (2.0 mL) was placed in a sealed pressure vessel (25 mL) containing a magnetic stirring bar. The tube was capped and stirred in a preheated oil bath at 130 C for 24 h. After the mixture was cooled to room temperature, the resulting solution was diluted with ethyl acetate (25 mL) and extracted with ethyl acetate (3 × 10 mL). The combined organic layers were dried over anhydrous Na2SO4, filtered. The filtrate was concentrated, and the residue was purified by column chromatography on SiO2 (petroleum ether / dichloromethane, 30:1) to give 1,3,5-triazines (82% yield). |
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