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CAS No. : | 60792-79-2 | MDL No. : | MFCD00012891 |
Formula : | C4H14Cl2N2O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | KTCUXFVANABSPX-UHFFFAOYSA-N |
M.W : | 177.07 | Pubchem ID : | 2829023 |
Synonyms : |
|
Chemical Name : | 2,2'-Oxybis(ethylamine) dihydrochloride |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 170℃; for 0.0833333h;Microwave irradiation; | A suspension of 0.2 M 2,2'-oxydiethylamine dihydrochloride (0.167 gm, 0.92 mmole) and 0.4 M DIEA (0.40 ml, 2.3 mmole) in 2.5 DMF was added to <strong>[6492-86-0]4-amino-1,8-naphthalic anhydride</strong> (0.067 gm, 0.30 mmole) and heated at 170 C with microwave treatment under nitrogen for 10 minutes. The mixture was cooled, concentrated under vacuum, and purified by preparatory HPLC to give N-aminoethylethoxy-4-amino- EPO <DP n="99"/>1,8 naphthalimide 8. MS m/z 300 (M + H)+ |
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