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CAS No. : | 5824-40-8 | MDL No. : | MFCD00008047 |
Formula : | C19H17N | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | BZVJOYBTLHNRDW-UHFFFAOYSA-N |
M.W : | 259.35 | Pubchem ID : | 138598 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
75% | With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 80℃; | In single-port bottle by adding triphenyl methylamine (2.32g, 8 . 95mmol), 2-chloro-methyl and oxazoline (1.50g, 8 . 95mmol), potassium carbonate (1.36g, 9 . 85mmol), potassium iodide (297 mg, 1 . 79mmol) and 25mLN, after N-dimethyl formamide, for 80 C lower reaction sleepovers. Water quenching the reaction, ethyl acetate extraction, combined with the phase, drying, filtering, evaporating solvent under reduced pressure. Residual oil-shaped column chromatography (silica gel, petroleum ether: ethyl acetate = 20:1) obtaining white transparent oily separation and purification (2.60g, 75%). |
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