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CAS No. : | 574-96-9 | MDL No. : | MFCD00092325 |
Formula : | C11H8O2 | Boiling Point : | No data available |
Linear Structure Formula : | C10H6(OH)CHO | InChI Key : | OITQDWKMIPXGFL-UHFFFAOYSA-N |
M.W : | 172.18 | Pubchem ID : | 443195 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313 | UN#: | |
Hazard Statements: | H315-H319 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
86% | In methanol; ethanol; for 24h;Reflux; | General procedure: To a solution of the amine (2.90 mmol) in ethanol (10 mL) was slowly added a solution of the corresponding aldehyde (2.90 mmol) in methanol (2 mL). The mixture was refluxed for 24 h and then cooled at room temperature. When a solid did not precipitate, the reaction mixture was evaporated under reduced pressure and gave rise to a solid on standing or on cooling. The resulting product was isolated by filtration, washed successively with cold water, ethanol, and diethyl ether, and recrystallized from ethanol or methanol. |
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