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CAS No. : | 53981-23-0 | MDL No. : | MFCD07368754 |
Formula : | C6H6FNO | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | QOZLOYKAFDTQNU-UHFFFAOYSA-N |
M.W : | 127.12 | Pubchem ID : | 2782778 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P262-P280-P301+P310-P304+P340-P305+P351+P338-P310 | UN#: | |
Hazard Statements: | H302-H312-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
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With sodium; boron tribromide; In methanol; n-heptane; dichloromethane; water; | i 2-Amino-3-fluorophenol To a stirred solution of <strong>[19064-24-5]2,6-difluoronitrobenzene</strong> (1100 mg, 6.9 mmol) in dry methanol (20 ml) was added a solution of sodium (180 mg, 7.8 mmol) in dry methanol (8 ml). The solution was stirred overnight. After concentration, water was added and the solution was extracted with ether, dried over MgSO4, filtered and concentrated to a yellow residue (870 mg.5.08 mmol). To the solution of the yellow residue in dichloromethane (10 ml) boron tribromide (1M in dichloromethane, 10 ml) was added and stirred at room temperature overnight. Water was then added and the solution stirred for further 60 min. The organic phase was separated and the water phase was extracted with ether. The combined organic phase were dried over MgSO4, filtered and concentrated in vacuo to give a brownish residue. The residue was taken up into ether and washed with 2M sodium hydroxide and water. The water and sodium hydroxide washings were combined and neutralised with 6M HCl and extracted with ether, dried over MgSO4 and evaporated to give a yellow residue which was purified by flash chromatography on silica gel with EtOAc:Heptane: 1:3 as eluant to give the product (720 mg, 4.6 mmol) which was directly suspended with palladium-charcoal (140 mg) in water-ethanol (30 ml). |