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[ CAS No. 53386-64-4 ] {[proInfo.proName]}

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Chemical Structure| 53386-64-4
Chemical Structure| 53386-64-4
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Product Details of [ 53386-64-4 ]

CAS No. :53386-64-4 MDL No. :MFCD03247461
Formula : C10H13NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :UAWVZBDVSNLPDT-UHFFFAOYSA-N
M.W : 179.22 Pubchem ID :422659
Synonyms :

Safety of [ 53386-64-4 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3265
Hazard Statements:H227-H314-H412 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 53386-64-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 53386-64-4 ]

[ 53386-64-4 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 5545-54-0 ]
  • [ 53386-64-4 ]
  • [ 1026719-79-8 ]
  • 2
  • [ 53386-64-4 ]
  • [ 119479-32-2 ]
  • [benzyl-(2-<i>tert</i>-butoxycarbonylamino-pent-4-enoyl)-amino]-acetic acid methyl ester [ No CAS ]
  • 3
  • [ 59237-53-5 ]
  • [ 53386-64-4 ]
  • [ 1236119-50-8 ]
YieldReaction ConditionsOperation in experiment
90% at 20 - 90℃;Neat (no solvent); Inert atmosphere; Methyl 6-chloro-5-nitronicotinate (2.0 g, 9.23 mmol) was added to methyl 2-(benzylamino)acetate (6.0 g, 31.05 mmol) neat while stirring at room temperature. The viscous yellow reaction was heated to 90° C. for one h and then allowed to cool back to room temperature. The reaction was diluted with dichloromethane (20 mL) and purified via column chromatography (220 g SiO2, 20-30percent gradient, ethyl acetate in hexanes) to yield the title compound (3.10 g, 90percent yield) as a yellow oil. [M+H] calc'd for C18H19N3O6, 374; found, 374.
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