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CAS No. : | 512-04-9 | MDL No. : | MFCD00016887 |
Formula : | C27H42O3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 414.62 | Pubchem ID : | - |
Synonyms : |
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Chemical Name : | (2'R,4S,5'R,6aR,6bS,8aS,8bR,9S,11aS,12aS,12bS)-5',6a,8a,9-Tetramethyl-1,3,3',4,4',5,5',6,6a,6b,6',7,8,8a,8b,9,11a,12,12a,12b-icosahydrospiro[naphtho[2',1':4,5]indeno[2,1-b]furan-10,2'-pyran]-4-ol |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
4 g | With diethylamine; In chloroform; at 20℃; for 12h; | Weigh 4.2g of diosgenin in 100mL of chloroform in a 500mL three-necked flask.Add 10 mL of diethylamine,2-methyl-3-trifluoromethylbenzyl bromide 3.0g,Stir, incubate at room temperature for 12h,HPLC (chromatographic conditions: Column: Agilent Zorbax SB-C18 (4.6mm × 150mm, 5um), mobile phase: acetonitrile-water (90:10), flow rate: 1.0mL.min-1, detection wavelength: 203nm, column temperature: 35 ) Detect the total reaction of diosgenin, evaporate chloroform to reduce the liquid volume to 1/4, cool to 5 and crystallize overnight, filter, HPLC track the reaction and separation and purification process of the product, and dry the solid at 60 for 4 h That is, 4.0 g of the product was obtained as a yellow powder. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
4.3 g | With diethylamine; In dichloromethane; at 40.0℃; for 8.0h; | Weigh 4.2 g of diosgenin in 100 mL of dichloromethane in a 500 mL three-necked flask.10 mL of diethylamine and 3.0 g of <strong>[261952-19-6]4-methyl-3-trifluoromethylbenzyl bromide</strong> were added,Stir, incubate at 40 C for 8h,HPLC (chromatographic conditions: Column: Agilent Zorbax SB-C18 (4.6mm × 150mm, 5um), mobile phase: acetonitrile-water (90:10), flow rate: 1.0mL.min-1, detection wavelength: 203nm, column temperature: 35 ) Detect the total reaction of diosgenin. Dichloromethane was distilled off until the liquid volume was reduced to 1/4. The solution was cooled to 5 and crystallized overnight.The separation and purification process of the reaction and product were followed by HPLC. The solid was dried at 60 C for 4h.This gave 4.3 g of product as a yellow powder. |