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CAS No. : | 498-07-7 | MDL No. : | MFCD00063248 |
Formula : | C6H10O5 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | TWNIBLMWSKIRAT-VFUOTHLCSA-N |
M.W : | 162.14 | Pubchem ID : | 2724705 |
Synonyms : |
1,6-Anhydro-β-D-glucopyranose;1,6-Anhydro-β-D-glucose
|
Chemical Name : | (1R,2S,3S,4R,5R)-6,8-Dioxabicyclo[3.2.1]octane-2,3,4-triol |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
34.4 g | With pyridine; Novozym 435; for 48h; | The compound shown in Formula 6 is dissolved in 1500 ml of pyridine and added to Novozym 435(immobilized Candida antarctica lipase) 20g,Acetic acid succinimide ester 47.2g, placed in a shaker controlled 30±1°C reaction for 48h,After filtration, the filtrate was concentrated to dryness under reduced pressure, dissolved in 500 ml of methylene chloride, washed with 500 ml of 1N diluted hydrochloric acid, and washed with 500 ml of water. The organic phases were combined, the organic phase was concentrated to dryness, 200 ml of toluene was added, and the mixture was stirred for 2 h. The solid precipitated and was filtered. drying,Formula 5The compound shown 34.4 g; |
A1269556[ 478518-93-3 ]
1,6-Anhydro-β-D-glucopyranose-13C6
Reason: Stable Isotope