Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 458532-96-2 | MDL No. : | MFCD03788416 |
Formula : | C5H5BClNO2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | WJYRVVDXJMJLTN-UHFFFAOYSA-N |
M.W : | 157.36 | Pubchem ID : | 5151595 |
Synonyms : |
|
Chemical Name : | (2-Chloropyridin-4-yl)boronic acid |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium carbonate;bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; water; at 100.0℃; for 16.0h; | To a solution of <strong>[886371-28-4]3-bromo-6-chloro-imidazo[1,2-a]pyridine</strong> (1 eq, 18.1 mmol, 4.2 g), 2- chloropyridin-4-yl boronic acid (1.05 eq, 19 mmol, 3 g), Na2COs (2 eq, 36.2 mmol, 3.84 g) in dioxane (30 ml) and water (10 ml), under an inert atmosphere of argon is added bis(triphenylphosphine)palladium II chloride (1.23 g). The reaction mixture is heated at 100 C for 16 hours. The mixture is diluted with H2O (50 ml) and extracted with EtOAc. The combined organic portions are washed with brine, dried (MgStheta4) and concentrated in vacuo. The residue is purified by flash chromatography on silica eluting with 0-50% EtOAc in iso-hexane to afford the title compound; [M+H]+ =264 (266). |
[ 1072951-54-2 ]
(2,6-Dichloropyridin-4-yl)boronic acid
Similarity: 0.84
[ 1003043-40-0 ]
(6-Chloro-5-methylpyridin-3-yl)boronic acid
Similarity: 0.73
[ 861905-97-7 ]
(2-Methylpyridin-4-yl)boronic acid hydrochloride
Similarity: 0.72
[ 458532-84-8 ]
2-Chloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine
Similarity: 0.72
[ 1072951-54-2 ]
(2,6-Dichloropyridin-4-yl)boronic acid
Similarity: 0.84
[ 1003043-40-0 ]
(6-Chloro-5-methylpyridin-3-yl)boronic acid
Similarity: 0.73
[ 458532-84-8 ]
2-Chloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine
Similarity: 0.72
[ 1070893-11-6 ]
(4,6-Dichloropyridine-3yl)boronic acid
Similarity: 0.70
[ 148493-34-9 ]
2,6-Dichloropyridin-3-ylboronic acid
Similarity: 0.68
[ 1072951-54-2 ]
(2,6-Dichloropyridin-4-yl)boronic acid
Similarity: 0.84
[ 1003043-40-0 ]
(6-Chloro-5-methylpyridin-3-yl)boronic acid
Similarity: 0.73
[ 861905-97-7 ]
(2-Methylpyridin-4-yl)boronic acid hydrochloride
Similarity: 0.72
[ 458532-84-8 ]
2-Chloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine
Similarity: 0.72