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CAS No. : | 4556-23-4 | MDL No. : | MFCD00006422 |
Formula : | C5H5NS | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | FHTDDANQIMVWKZ-UHFFFAOYSA-N |
M.W : | 111.16 | Pubchem ID : | 2723889 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
93% | With dihydrogen peroxide; In water; ethyl acetate; at 20℃; for 1.16667h;Green chemistry; | General procedure: In another study, a mixture of the VO-AMPD(at)SBA-15 (0.004 g), thiol (1 mmol) and H2O2 (0.4 mL) was stirred at room temperature in ethyl acetate (2 mL). The progress was monitored by TLC. After completion of the reaction, VO-AMPD(at)SBA-15 catalyst was separated from the mixture by filtration. Then products were extracted with ethyl acetate and dried, and the solvent was removed to give the pure disulfides. |