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CAS No. : | 3875-78-3 | MDL No. : | MFCD10698725 |
Formula : | C9H9BrO | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | KPFDABVKWKOIME-UHFFFAOYSA-N |
M.W : | 213.07 | Pubchem ID : | 10856814 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
82% | The mixture was stirred at room temperature for 3 h and then washed with water (20 ml) and brine (20 ml) and the organic layer separated, dried (MgSO4) and evaporated to a thick yellow oil, which was purified by column chromatography using 5% EtOAc in pentane to give the title product (1.3 g, 82%); 1H-NMR (400 MHz, CDCl3) delta: 1.90-1.98 (m, 2H), 2.73 (t, 2H), 4.14 (t, 2H), 6.61 (d, 1H), 7.08-7.15 (m, 2H). |
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