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CAS No. : | 364385-54-6 | MDL No. : | MFCD09952106 |
Formula : | C11H22N2O2 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | AKVIZYGPJIWKOS-DTWKUNHWSA-N |
M.W : | 214.30 | Pubchem ID : | 1514392 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313 | UN#: | |
Hazard Statements: | H315-H319 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With triethylamine; In dichloromethane; water; | Step 1 (1R,2S)-N-tert-Butoxycarbonyl-2-(2-chloro-6-methoxyquinazolin-4-yl)aminocyclohexylamine A solution of 710 mg of <strong>[105763-77-7]2,4-dichloro-6-methoxyquinazoline</strong> in 20 mL of methylene chloride was combined with 471 mg of triethylamine and 750 mg of (1S,2R)-2-tert-butoxycarbonylaminocyclohexylamine, and stirred at room temperature for 48 hours. After concentrating, the mixture was combined with water, extracted with methylene chloride, and dried. After solvent was distilled off, the residue was purified by column chromatography on silica gel (chloroform:methanol 20:1) to obtain 1.20 g of the desirable compound. |
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