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CAS No. : | 352535-82-1 | MDL No. : | MFCD05664224 |
Formula : | C6H5BClFO2 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | SUYRGLRWMPEARP-UHFFFAOYSA-N |
M.W : | 174.37 | Pubchem ID : | 16217158 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
79% | With bis(tri-t-butylphosphine)palladium(0); potassium carbonate; In tetrahydrofuran; water; for 1h;Heating; | <strong>[14381-51-2]3-bromobenzene-1,2-diol</strong> (50 g, 0.26 mol) and (3-chloro-2-fluorophenyl) boronic acid (46.1 g, 0.21 mol) were dissolved in 500 ml of tetrahydrofuran in a 2000 ml round- After dissolving, 1.5M aqueous potassium carbonate solution (400 ml) was added and bis (tri-tert-butylphosphine) palladium (0) (1.35 g, 2.36 mmol)Followed by heating and stirring for 1 hour. The reaction mixture was cooled to room temperature and the water layer was separated and removed. The organic layer was dried over anhydrous magnesium sulfate, concentrated under reduced pressure, recrystallized using hexane, and dried to obtain the compound of Formula 7-a (49.8 g, yield 79percent |
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