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[ CAS No. 347-91-1 ] {[proInfo.proName]}

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Chemical Structure| 347-91-1
Chemical Structure| 347-91-1
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Product Details of [ 347-91-1 ]

CAS No. :347-91-1 MDL No. :MFCD02260684
Formula : C14H11FO Boiling Point : -
Linear Structure Formula :- InChI Key :CWYRBOMWOQXYFZ-UHFFFAOYSA-N
M.W : 214.24 Pubchem ID :236329
Synonyms :

Safety of [ 347-91-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 347-91-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 347-91-1 ]

[ 347-91-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 71-43-2 ]
  • [ 459-04-1 ]
  • [ 347-91-1 ]
YieldReaction ConditionsOperation in experiment
97% aluminum (III) chloride; at 25 - 50℃; for 8.5h; 2- (4-Fluoro-phenyl)-1-phenyl-ethanone To a solution of benzene (182 mL) at 0 C was added AIC13 (46.4 g, 348 mmol). A portion of 4-fluorophenyl acetyl chloride (50.0 g, 290 mmol) was then added drop- wise over 30 min. Once the addition was complete, the reaction was allowed to warm to 25 C and then heated to 50 C for 8 hr. Subsequently, the reaction mixture was cooled to 25 C and poured onto ice (400 g). To the resulting suspension in ice was added 1.0 N HCI (50 mL). The organic layer was separated and washed with 10% HCI, saturated NaHC03 and brine. The organic layer was then dried and concentrated to afford a solid that was washed twice with hexane (200 mL) and then dried under vacuum to afford 2- (4-fluoro-phenyl)-1-phenyl-ethanone (59.90 g, 97%): MS (APCI+) : Sz 215.0 (M+H); H-NMR (CDCI3) o ?. 82 (d, 2 H), 7.54-7. 41 (m, 3 H), 7.22-7. 17 (m, 2 H), 7.00-6. 96 (m, 2 H), 4.23 (s, 3 H).
  • 2
  • [ 395-21-1 ]
  • [ 347-84-2 ]
  • [ 347-91-1 ]
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