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CAS No. : | 32974-92-8 | MDL No. : | MFCD00038028 |
Formula : | C8H10N2O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | PPJSYGVFDJEMRP-UHFFFAOYSA-N |
M.W : | 150.18 | Pubchem ID : | 61918 |
Synonyms : |
|
Chemical Name : | 1-(3-Ethylpyrazin-2-yl)ethanone |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
41% | With hydrogen bromide; bromine; In methanol; water; at 60℃; for 3h; | To a solution of 6 g (40 mmol) 1-(3-Ethyl-pyrazin-2-yl)-ethanone in 21 ml HBr (33%) and 7 ml methanol was added 2 ml (40 mmol) bromine and the mixture was heated to 60 C for 3 h. After removal of the volatiles under reduced pressure the residue was washed with diethyl ether and ethyl acetate. 6.4 g (41%) of the title compound was obtained as grey solid. MS (m/e): 229.1 (M+H, 100%). |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
at 130℃; for 2h; | Example 2522-(N-isopropyl-2-hydroxyethyl)aminoethyl-3-ethyl-2-pyrazylketone 8725 <strong>[32974-92-8]2-acetyl-3-ethylpyrazine</strong> (150 mg), isopropylethanol amine (103 mg), and paraformaldehyde (38 mg) were reacted at 130 C. for 2 hours.NMR (CDCl3) 1.30 (m, 6H), 2.73 (m, 2H), 3.14 (m, 2H), 3.9 (m, 2H), 4.25 (m, 2H), 8.4, 8.5TG 75.4 (3 vitriol) 42.9 (10 mumol) 17.7 (30 mumol)SOCE 0 (10 mumol) 0 (30 mumol) 0 (100 mumolIICR 0 (10 vitriol) 0 (30 mumol) 80 (100 mumol) |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In 1,4-dioxane; at 130℃; for 2h; | Example 1882-(N-t-butylbenzyl)aminoethyl-2-(3-ethyl)-pyrazylketone 8658 <strong>[32974-92-8]2-acetyl-3-ethylpyrazine</strong> (151 mg), benzyl-t-butyl amine (149 mg), and paraformaldehyde (40 mg) were reacted in dioxane (0.2 ml) at 130 C. for 2 hours.NMR (CDCl3) 1.1 (m, 9H), 2.7 (m, 1H), 3.1 (m, 4H), 3.7 (m, 2H), 7-7.1 (m, 1H), 8.5-8.6 (m, 1H)TG 42 (3 mumol) 22 (10 mumol) 10 (30 mumol)SOCE 0 (10 mumol) 0 (30 mumol) 20 (100 mumol)IICR 50 (10 mumol) 90 (30 mumol) 100 (100 mumol) |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In 1,4-dioxane; at 130℃; for 2h; | Example 1872-(N-hydroxyethylbenzyl)aminoethyl-2-(3-ethyl)-pyrazylketone 8657 <strong>[32974-92-8]2-acetyl-3-ethylpyrazine</strong> (150 mg), hydroxyethylisopropylamine (149 mg), and paraformaldehyde (40 mg) were reacted in dioxane (0.2 ml) at 130 C. for 2 hours.NMR (CDCl3) 1.3 (m, 3H), 2.6 (m, 4H), 3.2 (m, 4H), 8.6 (s, 1H), 8.7 (s, 1H)TG 90.3 (3 mumol) 73 (10 mumol) 30 (30 mumol)SOCE 0 (10 mumol) 0 (30 mumol) 10 (100 mumol)IICR 20 (10 mumol) 10 (30 mumol) 100 (100 mumol) |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
at 130℃; for 2h; | Example 2602-(N-bis-hydroxyethyl)aminoethyl-3-ethyl-2-pyrazylketone 8733 <strong>[32974-92-8]2-acetyl-3-ethylpyrazine</strong> (148 mg), diethanol amine (119 mg), and paraformaldehyde (40 mg) were reacted at 130 C. for 2 hours.NMR (CDCl3) 1.31 (t, 3H), 2.75 (m, 43H), 3.25 (m, 2H), 3.71 (m, 2H), 3.80 (M, 2H), 4.0 (m, 2H), 8.2 (s, 1H), 8.25 (s, 1H)TG 76.3 (3 mumol) 45.2 (10 mumol) 10.2 (30 mumol)SOCE 0 (10 mumol) 0 (30 mumol) 0 (100 mumol)IICR 20 (10 mumol) 0 (30 mumol) 20 (100 mumol) |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In 1,4-dioxane; at 130℃; for 2h; | Example 1862-(N-isopropylbenzyl)aminoethyl-2-(3-ethyl)-pyrazylketone 8656 <strong>[32974-92-8]2-acetyl-3-ethylpyrazine</strong> (151 mg), benzylisopropylamine (149 mg), and paraformaldehyde (40 mg) were reacted in dioxane (0.2 ml) at 130 C. for 2 hours.NMR (CDCl3) 1.1-1.2 (m, 6H), 2.7 (m, 1H), 3.1 (m, 4H), 3.7 (m, 2H), 7-7.2 (m, 1H)TG 29 (3 mumol) 16 (10 mumol) 14 (30 mumol)SOCE 0 (10 mumol) 0 (30 mumol) 10 (100 mumol)IICR 70 (10 mumol) 90 (30 mumol) 100 (100 mumol) |
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