Alternatived Products of [ 216959-34-1 ]
Product Details of [ 216959-34-1 ]
CAS No. : | 216959-34-1 |
MDL No. : | MFCD01631201 |
Formula : |
C9H15NO5
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | DSDQWJVXMDHQLK-UHFFFAOYSA-N |
M.W : |
217.22
|
Pubchem ID : | 2733665 |
Synonyms : |
|
Safety of [ 216959-34-1 ]
Application In Synthesis of [ 216959-34-1 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 216959-34-1 ]
- 1
-
[ 1046816-75-4 ]
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[ 216959-34-1 ]
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C14H18ClN3O5
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
60.01% |
With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -20 - 20℃; for 12h; |
Compound II-1 (50.01 g, 0.347 mol, 1.0 e.q.) was dissolved in THF (500 mL), and compound III (75.39 g, 0.347 mol, 1.0 e.q.) was added.Triphenylphosphine (135.1 g, 0.347 mol, 1.0 e.q.), cooled to -20 ° C, DIAD (70.21 g, 0.347 mol, 1.0 e.q.) was added dropwise, and the reaction was stirred at room temperature for 12 h.The reaction solution was poured into water, extracted with EA and washed with saturated aqueous sodium hydrogen carbonate.After drying, the reaction solution was concentrated, and the precipitated solid was removed by crystallization with PE/EA. The reaction solution was concentrated to give Compound IV-1 as a yellow liquid, 71.43 g. The yield was 60.01percent. |
- 2
-
[ 1046816-75-4 ]
-
[ 216959-34-1 ]
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tert-butyl ((2-chloropyrimidin-5-yl)methyl)carbamate
[ No CAS ]