Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 211235-87-9 | MDL No. : | MFCD01651767 |
Formula : | C8H6O4S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | OYWUVHMKKSZDJH-UHFFFAOYSA-N |
M.W : | 198.20 | Pubchem ID : | 3430937 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
43%; 22% | General procedure: To a 50 mL of Schlenk tube were added 1 or 3 (0.2 mmol, 1.0 equiv), Pd(OAc)2 (10 mol%), dppf (10 mol%) under air, followed by K3PO4·3H2O (0.3 mmol, 1.5 equiv) and Ag2CO3 (0.3 mmol, 1.5 equiv) . The mixture was then evacuated and back filled with N2 (3 times). Bromodichoromethane (0.4 mmol, 2.0 equiv), Ac2O (2 mmol, 190 uL) and CH3CN (1 mL) were added subsequently. The Schlenk tube was screw capped and put into a preheated oil bath (60 C). After stirring for 24 hours, the reaction mixture was cooled to room temperature, diluted with CH2Cl2 and Ethyl Acetate, then filtered with a pad of silica gel. The isolated yield was given by a hydrolysis pathway, in which the concentrated reaction mixture was diluted with 5 mL CH2Cl2 and 10 mL 3 N HCl and stirred over night. The reaction mixture was extracted with dichloromethane (3 times) and the solvent was removed under rotary evaporation. The residue was then purified by a preparative TLC to give product 2 or 4. |
[ 204905-77-1 ]
2,3-Dihydrothieno[3,4-b][1,4]dioxine-5-carbaldehyde
Similarity: 0.98
[ 852054-42-3 ]
7-Bromo-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbaldehyde
Similarity: 0.81
[ 67808-64-4 ]
Methyl 5-formylthiophene-2-carboxylate
Similarity: 0.63
[ 622864-56-6 ]
5-Methoxybenzo[b]thiophene-2-carbaldehyde
Similarity: 0.60
[ 4565-31-5 ]
5-Formylthiophene-2-carboxylic acid
Similarity: 0.60
[ 204905-77-1 ]
2,3-Dihydrothieno[3,4-b][1,4]dioxine-5-carbaldehyde
Similarity: 0.98
[ 852054-42-3 ]
7-Bromo-2,3-dihydrothieno[3,4-b][1,4]dioxine-5-carbaldehyde
Similarity: 0.81
[ 195602-17-6 ]
2,2',3,3'-Tetrahydro-5,5'-bithieno[3,4-b][1,4]dioxine
Similarity: 0.73
[ 146796-02-3 ]
(2,3-Dihydrothieno[3,4-b][1,4]dioxin-2-yl)methanol
Similarity: 0.59