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CAS No. : | 2040-04-2 | MDL No. : | MFCD00008729 |
Formula : | C10H12O3 | Boiling Point : | - |
Linear Structure Formula : | (CH3O)2C6H3COCH3 | InChI Key : | XEUGKOFTNAYMMX-UHFFFAOYSA-N |
M.W : | 180.20 | Pubchem ID : | 16267 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
50% | With iodine; In dimethyl sulfoxide; at 110℃; for 12h; | General procedure: DMSO (3 mL) was added to a mixture of acetophenone (1.0equiv.) and I2 (1.1 equiv.). The solutionwas stirred at 110 °C, then 2-aminobenzamide (1.0 equiv.) in 2mL DMSO was added dropwise tothe mixture during 1-2 h. After a complete disappearance of thestarting material, 50 mL water and 30 mL saturated brine wereadded to the mixture. The solution was extracted with CH2Cl2(50 mLx3). The organic layer was washed with 10percent Na2S2O3 solution, dried over anhydrous Na2SO4 and concentrated underreduced pressure. The residue was purified by silica gel chromatography(petroleum ether/EtOAc 5:1) to yield the desiredproducts 9a-9d. |
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