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CAS No. : | 20358-06-9 | MDL No. : | MFCD04448824 |
Formula : | C7H5FN2S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | CBVRCEFUXXJLSG-UHFFFAOYSA-N |
M.W : | 168.19 | Pubchem ID : | 2049887 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72% | To a suspension of (2-fluorophenyl) thiourea (1.7g, 10.0 mmol) in chloroform [(25ML)] was added a solution of bromine (0.51 mL; 10.0 mmol) dropwise at room temperature. The resulting mixture was heated under reflux for 3 hrs. The solvent was evaporated, water was added and the mixture was neutralized with ammonium hydroxide. The resulting white precipitation was collected by filtration and dried to yield 1.2 g (72%) of the title compound which was used in the subsequent step without further purification. |
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