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[ CAS No. 201046-59-5 ] {[proInfo.proName]}

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Chemical Structure| 201046-59-5
Chemical Structure| 201046-59-5
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Product Details of [ 201046-59-5 ]

CAS No. :201046-59-5 MDL No. :MFCD00153362
Formula : C35H32N2O6 Boiling Point : -
Linear Structure Formula :- InChI Key :HFKOCIWEYMAENQ-YTTGMZPUSA-N
M.W : 576.64 Pubchem ID :13783707
Synonyms :
Chemical Name :(S)-2,5-Bis((((9H-fluoren-9-yl)methoxy)carbonyl)amino)pentanoic acid

Safety of [ 201046-59-5 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 201046-59-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 201046-59-5 ]

[ 201046-59-5 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 96-09-3 ]
  • [ 2999-46-4 ]
  • [ 201046-59-5 ]
  • 2,5-bis-(9<i>H</i>-fluoren-9-ylmethoxycarbonylamino)-pentanoic acid 2-(ethoxycarbonylmethyl-carbamoyl)-2-phenyl-ethyl ester [ No CAS ]
  • 2
  • [ 745795-94-2 ]
  • [ 201046-59-5 ]
  • [ 745795-99-7 ]
  • 3
  • [ 70-26-8 ]
  • [ 28920-43-6 ]
  • [ 201046-59-5 ]
YieldReaction ConditionsOperation in experiment
79% EXAMPLE 53 Preparation of Nalpha,Ndelta-di-(9-Fluorenylmethoxycarbonyl)-L-ornithine (Compound No. 73) The reaction of 9-fluorenylmethyl chloroformate with L-ornithine according to the conditions described in example 2 provided the title product in 79% yield. 1H NMR (DMSO6): 1.42-1.80 (m, 4H), 3.00 (m, 2H), 3.94 (m, 1H), 4.20 (t, J=6.3, 2H), 4.29 (d, J=7.0, 4H), 7.28 (t, J=5.2, 1H), 7.30-7.48 (m, 8H), 7.63 (d, J=7.6, 1H), 7.67-7.73 (m, 4H), 7.88 (m, 4H), 12.50 (br s, 1H).
  • 4
  • [ 201046-59-5 ]
  • C5H12N3OPol [ No CAS ]
YieldReaction ConditionsOperation in experiment
General procedure: The procedure for the synthesis on Rink amide MBHA resin was identical to the synthesis on Cl-Trt resin except for the loading: Loading: The Fmoc protecting group from rink amide was removed by reaction with 20% piperidine in NMP (2 × 15 min, 5 mL each) and subsequent washing (2 × CH2Cl2, 2 × DMF, 5 mL each). Next, a preactivated solution of protected amino acid (0.78 mmol acid, 0.78 mmol, PyBOP, 2.34 mmol DIEA in 4.5 mL of DMF) was added to the resin and shaken for 2 h. The resin was washed with 2 × DMF and 2 × CH2Cl2 (3 mL each). Cleavage was performed as for Cl-Trt resin.
  • 5
  • [ 13094-51-4 ]
  • [ 872679-70-4 ]
  • C41H70NO7Pol [ No CAS ]
  • [ 201046-59-5 ]
  • (7S,34S)-1-bromo-7-(2-bromoacetamido)-34-carboxy-2,8,18,28,36-pentaoxo-12,15,22,25-tetraoxa-3,9,19,29,35-pentaazatripentacontan-53-oic acid [ No CAS ]
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