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CAS No. : | 2005-43-8 | MDL No. : | MFCD00234480 |
Formula : | C9H6BrN | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | QKJAZPHKNWSXDF-UHFFFAOYSA-N |
M.W : | 208.06 | Pubchem ID : | 2762756 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338-P310 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H332-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
42% | With bis(triphenylphosphine)nickel(II) chloride; potassium carbonate; In N,N-dimethyl-formamide; at 90℃; for 24h;Schlenk technique; Inert atmosphere; | Under a nitrogen atmosphere, bis(p-methoxyphenyl)phosphorus oxide (0.952g, 5mmol), 2-bromoquinoline (1.25g, 6mmol), K2CO3 (1.38g, 10mmol) were sequentially added to a 100mL Schlenk reaction flask. Ni(PPh3)Cl2 (159.3mg, 0.25mmol), DMF (5mL), and stirred at 90C for 24h. After the reaction, the mixture was diluted with water and extracted three times with ethyl acetate. The organic phase was washed with saturated sodium chloride solution, dried with anhydrous sodium sulfate, the mixture was chromatographed on silica gel column, eluted with petroleum ether/ethyl acetate=2:1, and drained to obtain a white solid (0.82g, 2.1mmol). The rate is 42%. |
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