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CAS No. : | 19764-30-8 | MDL No. : | MFCD00066069 |
Formula : | C8H15NO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | WXNXCEHXYPACJF-SSDOTTSWSA-N |
M.W : | 173.21 | Pubchem ID : | 1241420 |
Synonyms : |
N-Acetyl-R-leucine
|
Chemical Name : | Ac-D-Leu-OH |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In methanol; at 20℃; for 8h;Reflux; Inert atmosphere; | Compound 4c; (R)-1-(3-ethoxy-4-methoxyphenyl)-2-(methylsulfonyl)ethylamine'N-acetyl-D-leucine salt To a 100 ml of single-neck flask equipped with a magnetic stirrer, a reflux-condenser and an inert gas tube were added 1.365 g of compound 3a, 0.519 g of N-acetyl D-leucine, 10 ml of anhydrous methanol. The mixture was refluxed in an oil-bath for 1 hours, stirred for 3 hours at the room temperature, and filtered in vacuo to give 1.290 g of a white solid. The white solid was added in 10 ml of anhydrous methanol. The resultant mixture was refluxed for 1 hour, stirred for 3 hours at the room temperature, and filtered in vacuo to give 1.042 g of a white solid. |