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[ CAS No. 18362-64-6 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 18362-64-6
Chemical Structure| 18362-64-6
Structure of 18362-64-6 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 18362-64-6 ]

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Product Details of [ 18362-64-6 ]

CAS No. :18362-64-6 MDL No. :MFCD00015040
Formula : C9H16O2 Boiling Point : -
Linear Structure Formula :- InChI Key :CEGGECULKVTYMM-UHFFFAOYSA-N
M.W : 156.22 Pubchem ID :87597
Synonyms :

Safety of [ 18362-64-6 ]

Signal Word:Danger Class:3
Precautionary Statements:P261-P305+P351+P338 UN#:1224
Hazard Statements:H225-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 18362-64-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 18362-64-6 ]

[ 18362-64-6 ] Synthesis Path-Downstream   1~12

  • 1
  • [ 563-80-4 ]
  • [ 97-62-1 ]
  • [ 18362-64-6 ]
YieldReaction ConditionsOperation in experiment
77.3%Chromat. With potassium tert-butylate; In DMF (N,N-dimethyl-formamide); at 50℃; for 11h;Heating / reflux; In a 1-liter four-necked flask, 103 g of DMF and 1.33mol (149 g) of tert-butoxypotassium were placed, and theywere heated up to 50C with stirring by a mechanicalstirrer. Then, a liquid mixture consisting of 2.64 mol(307 g) of ethyl isobutyrate and 0.88 mol (75.6 g) of 3-methyl-2-butanone, was added by a dropping funnel over aperiod of 3 hours, followed by further stirring for 8hours under heating. It was confirmed by gaschromatography that 2,6-dimethyl-3,5-heptanedione was produced in an amount of 0.68 mol (107 g) in the solution(yield: 77.3% (based on 3-methylbutanone)).
  • 6
  • [ 18362-64-6 ]
  • [ 17536-00-4 ]
YieldReaction ConditionsOperation in experiment
100% With hydrazine; In ethanol; at 20℃; for 2h; Hydrazine (330 mg, 10 mmol) was added to a solution of 2,6-dimethylheptane-3,5- dione (1.6 g, 10 mmol) in ethanol (40 mL) at room temperature. After 2 hours, the reaction was concentrated in vacuo to afford 3, 5-diisopropyl-lH-pyrazole (1.5 g, 10 mmol, yield: 100%) which was used in the next step without further purification. MS: m/z 153.1 (M+H+).
  • 8
  • [ 5153-67-3 ]
  • [ 18362-64-6 ]
  • 3-isopropylcarbonyl-5-methyl-1-nitro-2-phenyl-4-hexanone [ No CAS ]
  • 9
  • [ 187737-37-7 ]
  • [ 18362-64-6 ]
  • 3-isobutyryl-2-isopropyl-5-methylfuran [ No CAS ]
  • 3-isopropylidene-2,6-dimethyl-3,5-heptanedione [ No CAS ]
  • 10
  • [ 74-85-1 ]
  • [ 18362-64-6 ]
  • 2,6-dimethyl-4-ethylidene-3,5-heptanedione [ No CAS ]
  • 11
  • [ 5162-44-7 ]
  • [ 18362-64-6 ]
  • 2,6,6-trimethyl-9-decene-3,5-dione [ No CAS ]
  • 12
  • [ 18362-64-6 ]
  • [ 91110-24-6 ]
  • 4-((3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl)-2,6-dimethyl-heptane-3,5-dione [ No CAS ]
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