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[ CAS No. 1755-15-3 ] {[proInfo.proName]}

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Chemical Structure| 1755-15-3
Chemical Structure| 1755-15-3
Structure of 1755-15-3 * Storage: {[proInfo.prStorage]}

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Product Details of [ 1755-15-3 ]

CAS No. :1755-15-3 MDL No. :MFCD00467663
Formula : C10H14O3 Boiling Point : -
Linear Structure Formula :- InChI Key :ITSKWKZDPHAQNK-UHFFFAOYSA-N
M.W : 182.22 Pubchem ID :519448
Synonyms :

Safety of [ 1755-15-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1755-15-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1755-15-3 ]

[ 1755-15-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1755-15-3 ]
  • [ 2799-07-7 ]
  • [ 216103-91-2 ]
  • 2
  • [ 64-17-5 ]
  • [ 1755-15-3 ]
  • [ 33906-30-8 ]
  • ethyl 2-(3,6,6-trimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indazol-1-yl)benzoate [ No CAS ]
YieldReaction ConditionsOperation in experiment
28% With hydrogenchloride; In water; for 6h;Reflux; 5.2.10 Ethyl 2-(3,6,6-trimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indazol-1-yl)benzoate (10) The reaction of <strong>[33906-30-8]2-hydrazinobenzoic acid hydrochloride</strong> (56.6 mg, 0.30 mmol) with 2-acetyl-5,5-dimethyl-1,3-cyclohexanedione (54.7 mg, 0.30 mmol) in ethanol (0.9 mL) under reflux for 6 h, by a procedure similar to that for 20 using concd HCl (0.30 mL) instead of H2SO4, gave ethyl 2-(3,6,6-trimethyl-4-oxo-4,5,6,7-tetrahydro-1H-indazol-1-yl)benzoate 10 (27.7 mg, 28%) as a powder. 1H NMR (CDCl3, 300 MHz) delta 8.01 (dd, J = 1.5, 7.5 Hz, 1H), 7.67-7.54 (m, 2H), 7.36 (dd, J = 1.5, 7.5 Hz, 1H), 4.15 (q, J = 7.2 Hz, 2H), 2.52 (s, 3H), 2.50 (s, 2H), 2.38 (s, 2H), 1.13 (t, J = 7.2 Hz, 3H), 1.09 (s, 6H); HRMS calcd for C19H23N2O3 (M+H) 327.1709, found 327.1703.
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