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[ CAS No. 17480-69-2 ] {[proInfo.proName]}

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Chemical Structure| 17480-69-2
Chemical Structure| 17480-69-2
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Product Details of [ 17480-69-2 ]

CAS No. :17480-69-2 MDL No. :MFCD00066325
Formula : C15H17N Boiling Point : -
Linear Structure Formula :HN(CH(CH3)C6H5)(CH2C6H5) InChI Key :ZYZHMSJNPCYUTB-ZDUSSCGKSA-N
M.W : 211.30 Pubchem ID :1268085
Synonyms :

Safety of [ 17480-69-2 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 17480-69-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 17480-69-2 ]

[ 17480-69-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 27829-72-7 ]
  • [ 17480-69-2 ]
  • (3R,1'S)-3-(N-α-methylbenzyl-N'-benzylamino)-hexanoate [ No CAS ]
  • [ 602275-62-7 ]
  • 2
  • [ 27829-72-7 ]
  • [ 17480-69-2 ]
  • [ 602275-62-7 ]
YieldReaction ConditionsOperation in experiment
50% With n-butyllithium; In tetrahydrofuran; at -78℃; for 1h; Example D: (S)-3-Amino-hexanoic acid ethyl ester <n="55"/>To a solution of (S)-(-)-N-benzyl-alpha-methyl-benzylamine (50 mL, 239 mmol) in THF (150 mL) at 00C is added nBuLi (2.5 M in THF) (100 mL, 250 mmol) under nitrogen atmosphere. The solution is cooled to -78°C and <strong>[27829-72-7]ethyl trans-2-hexenoate</strong> (16.6 g, 117 mmol) is added. The solution is stirred for 1 hour and saturated NH4Cl solution is added. The solution is warmed to room temperature and is extracted with EtOAc. The combined organic layer is dried with MgSO4 and is filtered. The filtrate is concentrated and the residue is purified by flash chromatography with 5percent EtOAc in Hexane as the eluent to afford the (S)-3-[Benzyl-((S)-l- phenyl-ethyl)-amino]-hexanoic acid ethyl ester (20.8 g, 50percent) as a colorless oil.
50% With n-butyllithium; In tetrahydrofuran; at -78 - 0℃; for 1h; To a solution of (S)-(-)-N-benzyl-alpha-methyl-benzylamme (50 mL, 239 mmol) m THF (150 mL) at 0 C was added BuLi (2.5 M m THF) (100 mL, 250 mmol) under nitrogen atmosphere. The solution was cooled to -78 C and <strong>[27829-72-7]ethyl trans-2-hexenoate</strong> (16.6 g, 117 mmol) was added. The solution was stirred for 1 hour and Sat. NH4Cl solution was added. The solution was warmed to room temperature and was extracted with EtOAc. The combined organic layer was dried with MgSO4 and was filtered. The filtrate was concentrated and the residue was purified by CombiFlash with 5percent EtOAc in Hexane as the eluent to afford the desirable product (S)-3- [Benzyl-((S)-l-phenyl-ethyl)-ammo]-hexanoic acid ethyl ester (20.8 g, 50percent) as a colorless oil.
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