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CAS No. : | 17364-16-8 | MDL No. : | MFCD00036904 |
Formula : | C24H50NO7P | Boiling Point : | - |
Linear Structure Formula : | CH3(CH2)14CO2CH2CHOHCH2OPO3CH2CH2N(CH3)3 | InChI Key : | ASWBNKHCZGQVJV-HSZRJFAPSA-N |
M.W : | 495.63 | Pubchem ID : | 460602 |
Synonyms : |
lyso-PPC;1-Palmitoyl-sn-glycero-3-phosphorylcholine
|
Chemical Name : | (R)-2-Hydroxy-3-(palmitoyloxy)propyl (2-(trimethylammonio)ethyl) phosphate |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
58% | With dmap; dicyclohexyl-carbodiimide; In chloroform; at 25℃; for 48h;Sonication; | To a suspension of 1-palmitoyl-2-hydroxy-sn-glycero-3-phos-phocholine 6 (0.5002 g, 1 mmol) in 25 mL of CHCl3 were addedFMOC-phe-gly-OH (0.5393 g, 1.2 mmol), DCC (0.2498 g, 1.2 mmol),DMAP (0.1479 g, 1.2 mmol) and 1 g of glass beads. The reaction wassonicated for 48 h at 25 C, the mixture was thenfiltered to removeDCC-urea and glass beads. The solvent was evaporated to one thirdof the volume and then loaded on a silica gel column forchromatography. A stepwise gradient of CHCl3/MeOH (5:1 and 5:2)was applied to elute DMAP and some impurities, followed byCHCl3/MeOH/H2O (65:25:4). The fractions corresponding to theproduct were combined, evaporated, re-dissolved in benzene andfreeze-dried to give 110 as a white solid (0.5352 g, 0.58 mmol, 58%).IR (Nujol): 3297 br m,1728 vs,1693 s,1654 vs,1536 m,1252 w cm1.1H NMR (CDCl3, 200 MHz) d 0.85 (br t, 3H), 1.25 (br s, 24H),1.50 (m, 2H), 2.20 (t, 2H, J = 6.7 Hz), 2.95 (m, 2H), 3.17 (br s, 9H), 3.67(br s, 2H), 3.95-4.30 (br m, 10H), 4.44 (m, 2H), 5.36 (m, 1H),6.15 (m, 1H), 7.21-7.47 (m, 11H), 7.72 (d, 2H, J = 7.4 Hz), 8.66 (m,1H).13C NMR (CDCl3, 50 MHz) d 14.28, 22.85, 24.92, 29.31, 29.52, 29.71,29.83, 29.87, 32.08, 34.04, 38.94, 41.47, 47.13, 54.34, 55.90, 59.63,62.44, 64.18, 66.28, 67.07, 71.96, 120.08, 125.27, 125.47, 126.94,127.26, 127.86, 128.57, 129.63, 137.05, 141.30, 143.90, 156.17, 169.83,172.39, 173.72. Rf (CHCl3/MeOH/H2O 65:25:4) 0.48. Anal. Cald forC50H72N3O11P2.5H2O C, 62.09; H, 8.02; N, 4.34; found: C, 62.33; H,8.03; N, 4.04. FAB-MS MH+ C50H72N3O11PH Calcd: 922.4977, found:922.4981. [a]D25 C -6.73 (c 0.98, CHCl3/MeOH 4:1). |