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CAS No. : | 16750-67-7 | MDL No. : | MFCD06656565 |
Formula : | C6H6BrNO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | CBQJZWGBFZAUEV-UHFFFAOYSA-N |
M.W : | 188.02 | Pubchem ID : | 14440265 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With iron; ammonium chloride; In methanol; water; | Example 191 3-{3-bromo-4-[3-(1-pyrrolidinyl)propoxy]phenyl}-2-methyl 5-(trifluoromethyl)-4(3H)-quinazolinone (1) Manufacture of 4-amino-2-bromophenol The target compound was obtained by reducing <strong>[5847-59-6]2-bromo-4-nitrophenol</strong> with iron in a mixed solution of methanol and ammonium chloride aqueous solution. <strong>[5847-59-6]2-bromo-4-nitrophenol</strong> was manufactured by the method described in the literature (J. Org. Chem., Vol. 62, 1997, p. 4504). | |
With sodium tetrahydroborate; In tetrahydrofuran; water; at 20℃; for 0.5h; | General procedure: A mixture of 3 mL of 0.015 mol L-1 aromatic nitro compound dissolved in tetrahydrofuran (THF), an aliquot of palladium nanoparticles, 300 muL of 2.0 mol L-1 NaCl solution and an aliquot of water were added into a reaction flask, totalizing 9 mL. Then, 900 muL of 0.5 mol L-1 NaBH4 solution freshly prepared was added to the above solution under continuous stirring. The final ratio H2O:THF was 2.3:1. The mixture was stirred at room temperature for 30 min. After this time, diethyl ether was added and the organic phase was separated and analyzed by gas chromatography (GC/MS) (chromatograph AgilentTechnologies model 7820A coupled to mass spectrometer Agilent Technologies model 5975, operating with acolumn HP5-ms). |