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[ CAS No. 1502-22-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 1502-22-3
Chemical Structure| 1502-22-3
Structure of 1502-22-3 * Storage: {[proInfo.prStorage]}

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Product Details of [ 1502-22-3 ]

CAS No. :1502-22-3 MDL No. :MFCD00013796
Formula : C12H18O Boiling Point : No data available
Linear Structure Formula :- InChI Key :GVNVAWHJIKLAGL-UHFFFAOYSA-N
M.W : 178.27 Pubchem ID :101175
Synonyms :

Safety of [ 1502-22-3 ]

Signal Word:Warning Class:
Precautionary Statements:P233-P260-P261-P264-P271-P280-P302+P352-P304-P304+P340-P305+P351+P338-P312-P321-P332+P313-P337+P313-P340-P362-P403-P403+P233-P405-P501 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1502-22-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1502-22-3 ]

[ 1502-22-3 ] Synthesis Path-Downstream   1~6

  • 4
  • [ 28746-99-8 ]
  • [ 1502-22-3 ]
  • [ 108-94-1 ]
  • 5
  • [ 108-94-1 ]
  • [ 1502-22-3 ]
  • [ 28746-99-8 ]
  • 6
  • [ 108-94-1 ]
  • [ 1502-22-3 ]
  • [ 1011-12-7 ]
  • [ 28746-99-8 ]
  • [ 52897-78-6 ]
  • C18H28O2 [ No CAS ]
  • C18H26O [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; at 20℃; for 72h; Dodecahydrotriphenylene (2). Calcined anhydrous sodiumhydroxide (6 g, 0.15 mol) was added to anhydrous freshly distilled cyclohexanone (60 mL, 0.58 mol) and the mixture obtained was stirred at room temperature for three days. Then, water (150 mL) was added to the reaction mixture with stirring, a precipitate was filtered off, washed with 10% aqueous HCl and water, and dried. The mixture of intermediate products without additional purification was added to polyphosphoric acid (40 g) and stirred for 2 h at 150 C. Then, the reaction mixture was mixed with anhydrous sodium sulfate (100 g), placed into a Soxhlet extractor, and the product was continuously extracted with light petroleum (b.p. 40-70 C). A precipitate was filtered off, washed with hexane, and dried. The yield was 24 g (52%),
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