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HazMat fee for 500 gram (Estimated)
Excepted Quantity
USD 0.00
Limited Quantity
USD 15-60
Inaccessible (Haz class 6.1), Domestic
USD 80+
Inaccessible (Haz class 6.1), International
USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic
USD 100+
Accessible (Haz class 3, 4, 5 or 8), International
USD 200+
Structure of 148-24-3 * Storage: {[proInfo.prStorage]}
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
General procedure: Cu (II) and Co (II) ions was synthesized by modifyingliterature methods8.1mmole of 8-hydroxyquinolinewas dissolved in alcoholic KOH. This solution wasadded drop wise to the solution of 1mmole metalsalt in alcohol. The reaction mixture was reuxedfor appropriate time. The solid product was obtainedafter completion of the reaction.The ligand 8-Hydroxyquinoline with Ni (II),Cu (II) and Co (II) ions was synthesized by modifyingliterature methods8.1mmole of 8-hydroxyquinolinewas dissolved in alcoholic KOH. This solution wasadded drop wise to the solution of 1mmole metalsalt in alcohol. The reaction mixture was reuxedfor appropriate time. The solid product was obtainedafter completion of the reaction.
Reference：
[1] Journal of Medicinal Chemistry, 2012, vol. 55, # 23, p. 10448 - 10459
[2] Oriental Journal of Chemistry, 2016, vol. 32, # 6, p. 2999 - 3013
[3] Chemische Berichte, 1985, vol. 118, # 4, p. 1556 - 1563
3
[ 148-24-3 ]
[ 6046-93-1 ]
[ 10380-28-6 ]
Reference：
[1] Journal of Solid State Chemistry, 1993, vol. 106, p. 451 - 460
[2] Canadian Journal of Chemistry, 1983, vol. 61, p. 2154 - 2158
[3] Research on Chemical Intermediates, 2015, vol. 41, # 8, p. 5703 - 5712
4
[ 148-24-3 ]
[ 10380-28-6 ]
Reference：
[1] Journal of the American Chemical Society, 1957, vol. 79, p. 4041
[2] Gmelin Handbuch, Gmelin Handbook: Cu: MVol.B4, 116, page 1696 - 1699,
5
[ 148-24-3 ]
[ 10380-28-6 ]
Reference：
[1] Theoretical and Experimental Chemistry, 1989, vol. 25, p. 97 - 101[2] Teoreticheskaya i Eksperimental'naya Khimiya, 1989, vol. 25, p. 108 - 112
[3] Industrial and Engineering Chemistry, Analytical Edition, 1943, vol. 15, p. 346 - 349
[4] Analyst (Cambridge, United Kingdom), 1933, vol. 58, p. 388 - 395
[5] , 1937, vol. 26, p. 391 - 413
[6] Gmelin Handbuch, Gmelin Handbook: Cu: MVol.B4, 116, page 1696 - 1699,
[7] Gmelin Handbuch, Gmelin Handbook: Cu: MVol.B4, 116, page 1696 - 1699,
6
[ 148-24-3 ]
[ 142-71-2 ]
[ 10380-28-6 ]
Reference：
[1] Kinetics and Catalysis, 1985, vol. 26, p. 50 - 57[2] Kinetika i Kataliz, 1985, vol. 26, p. 61 - 68
[3] Gazzetta Chimica Italiana, 1923, vol. 53, p. 605 - 616
[4] Monatshefte fuer Chemie, [5] Monatshefte fuer Chemie, 1882, vol. 3, p. 531 - 569
[6] Gmelin Handbuch, Gmelin Handbook: Cu: MVol.B4, 116, page 1696 - 1699,
[7] Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1990, vol. 29, # 5, p. 454 - 457
7
[ 148-24-3 ]
[ 10380-28-6 ]
Reference：
[1] Bulletin of the Chemical Society of Japan, 1988, vol. 61, # 5, p. 1761 - 1766
[2] Zeitschrift fuer Naturforschung, Teil B: Chemical Sciences, [3] Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995, vol. 50, p. 524 - 528
[4] Zeitschrift fuer Naturforschung, Teil B: Chemical Sciences, [5] Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995, vol. 50, p. 524 - 528
8
[ 148-24-3 ]
[ 10380-28-6 ]
Reference：
[1] Zeitschrift fuer Naturforschung, Teil B: Chemical Sciences, [2] Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995, vol. 50, p. 524 - 528
[3] Spectrochimica Acta, 1956, vol. 8, p. 1 - 8
[4] Zeitschrift fuer Naturforschung, Teil B: Chemical Sciences, [5] Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995, vol. 50, p. 524 - 528
[6] Gmelin Handbuch, Gmelin Handbook: Cu: MVol.B4, 116, page 1696 - 1699,
9
[ 148-24-3 ]
[ 10380-28-6 ]
Reference：
[1] Zeitschrift fuer Naturforschung, Teil B: Chemical Sciences, [2] Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995, vol. 50, p. 524 - 528
[3] Spectrochimica Acta, 1956, vol. 8, p. 1 - 8
[4] Zeitschrift fuer Naturforschung, Teil B: Chemical Sciences, [5] Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995, vol. 50, p. 524 - 528
[6] Gmelin Handbuch, Gmelin Handbook: Cu: MVol.B4, 116, page 1696 - 1699,
Compound according to Example 15 7-(Morpholin-4-yl-pyrazin-2-yl-methyl)-quinolin-8-ol The preparation was carried out analogously to the method described for Example Compound 6 using: 8-hydroxyquinoline (145 mg, 1.0 mmol) pyrazine-2-carbaldehyde (108 mg, 1.0 mmol) and morpholine (79 mul, 0.9 mmol) in dioxane (2 ml). Purification was carried out by means of preparative HPLC to give Example Compound 15 (91 mg, 28percent).
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