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[ CAS No. 13570-00-8 ] {[proInfo.proName]}

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Chemical Structure| 13570-00-8
Chemical Structure| 13570-00-8
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Product Details of [ 13570-00-8 ]

CAS No. :13570-00-8 MDL No. :MFCD08458369
Formula : C8H7N3 Boiling Point : No data available
Linear Structure Formula :- InChI Key :ZQZJULZPQACTES-UHFFFAOYSA-N
M.W : 145.16 Pubchem ID :12395500
Synonyms :

Safety of [ 13570-00-8 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 13570-00-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13570-00-8 ]

[ 13570-00-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 13570-00-8 ]
  • [ 85482-13-9 ]
  • 3-(1-(2,5-dichlorobenzyl)-1H-imidazol-2-yl)pyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
12.49 g With potassium carbonate; In N,N-dimethyl-formamide; at 20℃; for 7h; (1) In DMF (70 mE) was dissolved 3-(1H-imidazol-2-yl) pyridine (10 g, 68.9 mmol) which is publicly known through publication, potassium carbonate (19 g, 138 mmol) and 2,5- dichlorobenzyl bromide (19.83 g, 83 mmol) were added thereto, and the mixture was stirred at room temperature for 7 hours. After the reaction, water was added and the mixture was extracted twice with ethyl acetate (100 mE). Afier being washed with saturated aqueous sodium chloride, the organic layer was dried over anhydrous sodium sulfate. After concentrating the organic layer, the residue was purified by column chromatography to obtain 3-O-(2,5-dichlorobenzyl)- 1 H-imidazol-2-yl)pyridine (12.49 g):10189] ?H-NMR (DMSO-d5) oe: 8.71 (1H, d, J=2.0 Hz),8.58 (1H, dd, J=4.9, 1.5 Hz), 7.92 (1H, dt, J=8.1, 2.0 Hz),7.52-7.36 (4H, m), 7.15 (1H, d, J=1.5 Hz), 6.81 (1H, d, J=2.4 Hz), 5.41 (2H, s);10190] ESI-MS mlz=304 (M+H).
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