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[ CAS No. 135065-71-3 ] {[proInfo.proName]}

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Chemical Structure| 135065-71-3
Chemical Structure| 135065-71-3
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Product Details of [ 135065-71-3 ]

CAS No. :135065-71-3 MDL No. :MFCD09260605
Formula : C10H19NO4 Boiling Point : -
Linear Structure Formula :- InChI Key :FJYBLMJHXRWDAQ-MRVPVSSYSA-N
M.W : 217.26 Pubchem ID :1512576
Synonyms :

Safety of [ 135065-71-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 135065-71-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 135065-71-3 ]

[ 135065-71-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 135065-71-3 ]
  • [ 4983-28-2 ]
  • (R)-tert-butyl 2-(((2-chloropyrimidin-5-yl)oxy)methyl)morpholine-4-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
89% With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20℃; for 5h;Inert atmosphere; To a solution of (R)-tert-butyl 2-(hydroxymethyl)morpholine-4-carboxylate (605 mg, 2.79 mmol) in THF (5 mL) was added <strong>[4983-28-2]2-chloropyrimidin-5-ol</strong> (200 mg, 1.532 mmol), triphenylphosphine (548 mg, 2.089 mmol) and DIAD (0.406 mL, 2.089 mmol) and the reaction was stirred at 20 °C under an atmosphere of nitrogen for 5 hours. The reaction was concentrated and resuspended in 1 mL DMSO, then was subjected directly to purification by flash chromatography (60g pre-packed C-18 SNAP cartridge: 35percent to 90percent acetonitrile (0.1percent formic acid) in water (0.1percent formic acid)). The desired fractions were combined and concentrated to afford the title compound (410 mg, 1.24 mmol, 89 percent yield). LCMS Method A RT= 1.01 min, ES+ve 274 (M+H-tBu).
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