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CAS No. : | 131002-09-0 | MDL No. : | MFCD07700290 |
Formula : | C9H6ClNO | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | AVLGVJHAZWURPZ-UHFFFAOYSA-N |
M.W : | 179.60 | Pubchem ID : | 21779697 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
70% | With silver hexafluoroantimonate; In 1,2-dichloro-ethane; at 90℃; for 10h;High pressure; | 6-chloroisoquinolin-1 (2Eta)-one (12 mmol), bis(2-fluorophenyl)disulfide (10 mmol), hexafluoroantimonic acid were sequentially added to a pressure-resistant reaction tube at room temperature. Silver (10 mmol) and dichloroethane (6 mL). The reaction mixture was then reacted at 90 C for 10 hours. The reaction was stopped, concentrated under reduced pressure to give a crude material, which was washed with a mixture of petroleum ether and ethyl acetate. 4-(2-Fluorophenylthio)-6-chloroisoquinolin-1 (2H)-one. Yield 70%; |
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