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[ CAS No. 13031-76-0 ] {[proInfo.proName]}

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Chemical Structure| 13031-76-0
Chemical Structure| 13031-76-0
Structure of 13031-76-0 * Storage: {[proInfo.prStorage]}

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Product Details of [ 13031-76-0 ]

CAS No. :13031-76-0 MDL No. :MFCD00154867
Formula : C4H8O3S Boiling Point : No data available
Linear Structure Formula :- InChI Key :AMXKVIWWXBYXRS-UHFFFAOYSA-N
M.W : 136.17 Pubchem ID :98932
Synonyms :

Safety of [ 13031-76-0 ]

Signal Word:Warning Class:
Precautionary Statements:P280-P305+P351+P338 UN#:
Hazard Statements:H302 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 13031-76-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13031-76-0 ]

[ 13031-76-0 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 76924-19-1 ]
  • [ 1192-16-1 ]
  • [ 13031-76-0 ]
  • 2
  • [ 13031-76-0 ]
  • [ 17115-51-4 ]
YieldReaction ConditionsOperation in experiment
With manganese(II) oxide; In dichloromethane; at 20℃; for 16h; Mn02 (35 equiv, 2.2 g) was added to the alcohol (1 equiv, 100 mg) in DCM (20 mL) and the reaction was stirred at room temperature for 16 h. The reaction mixture was filtered and concentrated in vacuo. The residue was used in the next step without further purification
  • 3
  • [ 76924-20-4 ]
  • [ 1192-16-1 ]
  • [ 20627-66-1 ]
  • [ 13031-76-0 ]
  • 5
  • jones reagent [ No CAS ]
  • [ 13031-76-0 ]
  • [ 17115-51-4 ]
YieldReaction ConditionsOperation in experiment
In acetone; EXAMPLE 10C Tetrahydrothiophene-3-one-1,1-dioxide A mechanically stirred solution of the crude product from Example 10B in acetone (300 mL) was treated with Jones reagent (2.7M, 30 mL total) in portions over 2 hours until the brown color persisted, stirred for 1 hour, treated slowly with isopropyl alcohol (7.5 mL), stirred for 15 minutes, diluted with acetone (400 mL) and filtered through celite to remove the chromium salts. The filtrate was concentrated and purified by chromatography on silica gel (1:1 hexane:ethyl acetate) to provide 5.88 g of the title compound. 1H NMR (CDCl3) δ 3.08 (t, 2H), 3.58 (t, 2H), 3.70 (s, 2H).
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