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[ CAS No. 1168135-03-2 ] {[proInfo.proName]}

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Chemical Structure| 1168135-03-2
Chemical Structure| 1168135-03-2
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Product Details of [ 1168135-03-2 ]

CAS No. :1168135-03-2 MDL No. :MFCD11867874
Formula : C12H15BN2O2S Boiling Point : -
Linear Structure Formula :- InChI Key :KISHNZJGTMYYKH-UHFFFAOYSA-N
M.W : 262.14 Pubchem ID :46738015
Synonyms :

Safety of [ 1168135-03-2 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1168135-03-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1168135-03-2 ]

[ 1168135-03-2 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 1753-75-9 ]
  • [ 1168135-03-2 ]
YieldReaction ConditionsOperation in experiment
With potassium acetate; In N,N-dimethyl-formamide; Preparation 44 5-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazole Dichloro[1,1'-bis(diphenylphosphino)ferrocene]-palladium(II) (100 mg, 0.14 mmol, 0.03), potassium acetate (1.4 g, 14 mmol), and diboron bis(pinocol) ester (1.2 g, 4.7 mmol) were sequentially added to a stirred solution of <strong>[1753-75-9]5-bromobenzo[c][1,2,5]thiadiazole</strong> (1.0 g, 4.7 mmol) in N,N-dimethylformamide (12 mL) at 23 C. The resulting dark brown mixture was sealed under nitrogen, heated to 80 C., and stirred for 24 h. The cooled reaction mixture was diluted with water (500 mL) and extracted with diethyl ether (4*100 mL). The combined organic layers were diluted with hexane (100 mL) and washed with water (1*200 mL). The organic layer was dried (magnesium sulfate), gravity filtered, and concentrated by rotary evaporation to afford the title compound as a brown powder (960 mg, 80% yield): IR (KBr thin film) 2977 (m), 2930 (w), 1607 (w), 1471 (m) cm-1; 1H NMR (400 MHz, CDCl3) delta 8.54 (s, 1H), 7.93-8.01 (m, 2H), 1.40 (s, 12H).
  • 2
  • [ 1753-75-9 ]
  • [ 61676-62-8 ]
  • [ 1168135-03-2 ]
  • 3
  • [ 1753-75-9 ]
  • [ 73183-34-3 ]
  • [ 1168135-03-2 ]
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Related Functional Groups of
[ 1168135-03-2 ]

Organoboron

Chemical Structure| 1088118-97-1

[ 1088118-97-1 ]

4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazole

Similarity: 0.92

Related Parent Nucleus of
[ 1168135-03-2 ]

Other Aromatic Heterocycles

Chemical Structure| 1088118-97-1

[ 1088118-97-1 ]

4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)benzo[c][1,2,5]thiadiazole

Similarity: 0.92

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