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CAS No. : | 105627-79-0 | MDL No. : | MFCD08272853 |
Formula : | C9H7Cl2NO2S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | GZQNTWHQJJVIAK-UHFFFAOYSA-N |
M.W : | 264.13 | Pubchem ID : | 13116932 |
Synonyms : |
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Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P260-P280-P303+P361+P353-P301+P330+P331-P304+P340+P310-P305+P351+P338+P310 | UN#: | 3261 |
Hazard Statements: | H314 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
86% | With triethylamine; In dichloromethane; at 0℃; | To a solution of <strong>[127294-75-1]3-aminopiperidine dihydrochloride</strong> (50 mg, 0.29 mmol) and triethylamine (0.14 ml, 1 mmol) in dichloromethane (5 ml) was added in small portions isoquinolin-5-ylsulphonyl chloride hydrochloride (64 mg, 0.28 mmol) with stirring and ice-cooling. Water (10 ml) was added to the reaction mixture after stirring overnight. The organic layer was separated and washed twice with water, dried (MGSO4) and concentrated in vacuo. The crude product was purified by flash silica column eluting with 10% methanol in dichloromethane to afford the target compound as a white solid (71 mg, 0.24 mmol, 86%). Characterising Data: (CL4HL7N302S) : MS (ESI) m/z 292.2 [(M+H) +], 1H NMR (CD30D, 250 MHz) 8 1.13-1. 23 (M, 1H), 1.47-1. 65 (M, 1H), 1.75-1. 89 (m, 2H), 2.41-2. 49 (m, 1H), 2.64- 2.86 (M, 2H), 3.59-3. 78 (m, 2H), 7.88 (t, J= 8 Hz, 1H), 8.46 (d, J= 8 Hz, 1H), 8.47 (DD, J= 5 Hz AND J= 2 Hz, 1H), 8. 62 (D, J= 8 Hz, 1H), 8.64 (d, J= 8 Hz, 1H), 9.42 (s, 1H). |