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CAS No. : | 104-42-7 | MDL No. : | MFCD00007919 |
Formula : | C18H31N | Boiling Point : | No data available |
Linear Structure Formula : | CH3(CH2)11C6H4NH2 | InChI Key : | KLPPPIIIEMUEGP-UHFFFAOYSA-N |
M.W : | 261.45 | Pubchem ID : | 7701 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With toluene-4-sulfonic acid; at 203℃; for 4h;Dean-Stark; | A 50 mL three-neck flask equipped with an overhead stirrer, thermocouple, and a Dean-Stark trap topped by a spiral condenser was charged with 16.7 g dodecyl aniline, 10.3 g 4-hexylresorcinol, and 0.8 g p-toluene sulfonic acid. The reaction was stirred at 203 C. for 4 h. The product was taken up in xylenes, extracted with aqueous sodium bicarbonate, and washed with water. Volatiles were removed by rotary evaporation, followed by vacuum distillation to yield the product as a dark orange oil. |