N-Iodosuccinimide NEW
| Price | Get Latest Price |
| Package | 25KG |
| Min. Order: | 1KG |
| Supply Ability: | 50000KG/month |
| Update Time: | 2023-09-12 |
Product Details
| Product Name: N-Iodosuccinimide | CAS No.: 516-12-1 |
| EC-No.: 208-221-6 | Min. Order: 1KG |
| Purity: 99% | Supply Ability: 50000KG/month |
| Release date: 2023/09/12 |
| CAS: | 516-12-1 |
| MF: | C4H4INO2 |
| MW: | 224.98 |
| EINECS: | 208-221-6 |
| Product Categories: | C-X Bond Formation (Halogen);Synthetic Reagents;Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts;API intermediates;Biochemistry;Halogenation;Iodination;N-Substituted Maleimides, Succinimides & Phthalimides;N-Substituted Succinimides;Reagents for Oligosaccharide Synthesis;Synthetic Organic Chemistry;516-12-1;bc0001 |
| Mol File: | 516-12-1.mol |
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| N-Iodosuccinimide Chemical Properties |
| Melting point | 202-206 °C(lit.) |
| Boiling point | 249.6±23.0 °C(Predicted) |
| density | 2,245 g/cm3 |
| storage temp. | 2-8°C |
| solubility | Soluble in dioxane, tetrahydrfuran and acetonitrile. Insoluble in ether and carbon tetrachloride. |
| form | Crystalline Powder |
| pka | -2.57±0.20(Predicted) |
| color | White-yellow to brown |
| Water Solubility | decomposes |
| Sensitive | Moisture Sensitive |
| Merck | 14,5045 |
| BRN | 113917 |
| Stability: | Moisture Sensitive |
| InChIKey | LQZMLBORDGWNPD-UHFFFAOYSA-N |
| CAS DataBase Reference | 516-12-1(CAS DataBase Reference) |
| N-Iodosuccinimide Usage And Synthesis |
| Chemical Properties | white-yellow to brown crystalline powder |
| Uses | N-Iodosuccinimide is a iodo substituted succinimide that is used as an iodinating agent in chemical synthesis. |
| Uses | Iodination of ketones and aldehydes. Highly substituted iodobenzenes prepared via an efficient 2-step process from 1,6-diynes. Used with TFA to chemoselectively hydrolyze thioglycosides to 1-hydroxyglycosides. Synthesis of vinyl sulfones from olefins and benzenesulfinic acid. |
| Uses | N-Iodosuccinimide is used in the preparation of vinyl sulfones from olefins and benzenesulfinic acid. It acts as a source for I+ and involved in Hunsdiecker reactions for the conversion of cinnamic acids, and propiolic acids to the corresponding alfa-halostyrenes and 1-halo-1-alkynes respectively. It is also used to hydrolyze thioglycosides to 1-hydroxyglycosides with triluoroacetic acid. It is involved in the preparation of iodobenzene from 1,6-diynes. Further, it acts as an iodinating agent in chemical synthesis. |
| Preparation | To a solution of 39.2g of succinimide in 1200ml of boiling water was added 51.0g of freshly precipitated silver oxide, the mixture was filtered and the silver salt was allowed to crystallize. Filtration and washing with cold water furnished 45.0g of the silver salt of succinimide suitable for the iodination step. The finely powdered salt (49.5g) was added in portions with stirring to a solution of 50.8g of iodine in 300ml of acetone, the temperature being maintained at 5-10°C. After decolorization (30 min.), the silver iodide was filtered, the solvent was removed under reduced pressure at room temperature and the residue was washed with ether, yielding 43g of N-iodosuccinimide with mp 189-191°C. An analytical sample (85% recovery) was obtained by dissolving in the minimum quantity of hot dioxane and precipitating with carbon tetrachloride; colorless needles, mp 200-201°C. Ref: JACS 75, 3493 (1953) |
| Definition | ChEBI: N-iodosuccinimide is a five-membered cyclic dicarboximide compound having an iodo substituent on the nitrogen atom. It is a dicarboximide and a pyrrolidinone. It derives from a succinimide. |
Packing &shipping&Payment
Packing:25kg/drum
Shipping:by sea or by air
Payment:T/T,western union,moneygram
Packaging Details drum
Port:Tianjin
Lead Time :
Shipping:by sea or by air
Payment:T/T,western union,moneygram
Packaging Details drum
Port:Tianjin
Lead Time :
| Quantity(Kilograms) | 1 - 10000 | >10000 |
| Est. Time(days) | 5 | To be negotiated |
Company information
Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in 4'-Methylacetophenone,Levamisole hydrochloride ,N-Methylformamide and other chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big customers come from Europe, America and other countries in the world, we can guarantee the quality and price. In recent decades, with the efforts of all employees, we have established many cooperative companies in shandong, henan, guangdong and other places. Our corporate purpose is based on the market, enhance the strength, take the road of scientific and environmental sustainable development, relying on the country. Technology r & d center, increase the investment in r & d, based on the domestic market, expand the international market, manufacturing quality products, sincere service to the society, into a modern, ecological, scientific and technological enterprise world.
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