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ChemicalBook >> CAS DataBase List >>2-Chloro-N,N-dimethylacetamide

2-Chloro-N,N-dimethylacetamide

CAS No.
2675-89-0
Chemical Name:
2-Chloro-N,N-dimethylacetamide
Synonyms
EOS-61825;AKOS BBS-00000943;2-Chloro-N,N-dimethy;CHLOROACETYLDIMETHYLAMINE;N,N-DIMETHYLCHOROACETAMIDE;N,N-DIMETHYLCHLOROACETAMIDE;N-DiMethyl-2-chloroacetaMide;N,N-DIMETHYL-2-CHLOROACETAMIDE;2-CHLORO-N,N-DIMETHYLACETAMIDE;2-CHLORO-N,N-DIMETHYL ACETAMINE
CBNumber:
CB2343589
Molecular Formula:
C4H8ClNO
Molecular Weight:
121.57
MDL Number:
MFCD00039360
MOL File:
2675-89-0.mol
MSDS File:
SDS
Last updated:2024-11-26 17:46:08

2-Chloro-N,N-dimethylacetamide Properties

Melting point 15-16 °C
Boiling point 98-100°C/11mm
Density 1.182 g/mL at 20 °C (lit.)
refractive index n20/D 1.479
Flash point 98-100°C/11mm
storage temp. Store below +30°C.
solubility Chloroform (Slightly), Hexane (Slightly), Methanol (Slightly)
pka -0.95±0.70(Predicted)
form Liquid
color Clear colorless to pale yellow
BRN 969568
InChIKey XBPPLECAZBTMMK-UHFFFAOYSA-N
CAS DataBase Reference 2675-89-0(CAS DataBase Reference)
FDA UNII 7W3TRD462F

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictogramsGHS hazard pictograms
GHS05,GHS07
Signal word  Danger
Hazard statements  H302-H314
Precautionary statements  P270-P280-P301+P312-P303+P361+P353-P304+P340+P310-P305+P351+P338
Hazard Codes  C
Risk Statements  22-34
Safety Statements  26-36/37/39-45
RIDADR  UN 3265 8/PG 3
WGK Germany  3
HS Code  29241990
NFPA 704
1
3 0

2-Chloro-N,N-dimethylacetamide price More Price(32)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 24350 2-Chloro-N,N-dimethylacetamide ≥97.0% (GC) 2675-89-0 25mL $138 2024-03-01 Buy
TCI Chemical C3011 2-Chloro-N,N-dimethylacetamide 2675-89-0 5G $44 2024-03-01 Buy
TCI Chemical C3011 2-Chloro-N,N-dimethylacetamide 2675-89-0 25G $150 2024-03-01 Buy
Alfa Aesar H50229 2-Chloro-N,N-dimethylacetamide, 97% 2675-89-0 250mg $69.65 2024-03-01 Buy
Alfa Aesar H50229 2-Chloro-N,N-dimethylacetamide, 97% 2675-89-0 1g $226.65 2024-03-01 Buy
Product number Packaging Price Buy
24350 25mL $138 Buy
C3011 5G $44 Buy
C3011 25G $150 Buy
H50229 250mg $69.65 Buy
H50229 1g $226.65 Buy

2-Chloro-N,N-dimethylacetamide Chemical Properties,Uses,Production

Uses

2-Chloro-N,N-dimethylacetamide is N,M-dialkyl amide used as an organic catalyst in the preparation of phosphorylated thiosemicarbazide.

Uses

2-Chloro-N,N-dimethylacetamide (N,N-dimethylchloroacetamide) was used in the synthesis of (S)-carbinoxamine.

Synthesis

In a 500 mL four-necked flask, sodium hydrogen carbonate 126.0 g (1.50 mol) and 146.8 g of toluene were added, and the mixture was stirred while cooling. The internal temperature was maintained below 5 ° C, 112.9 g (1.00 mol) of chloroacetyl chloride was added dropwise over 4 hours, and 49.6 g (1.10 mol) of dimethylamine gas was blown over 4 hours. After stirring at -2 to 1 ° C. for 1 hour, the reaction solution was filtrated under reduced pressure to remove inorganic salt crystals by filtration. The crystals were washed with 100 g of toluene, and the filtrate and washings were combined. After separating and removing the aqueous layer in the filtrate washings, the toluene layer was concentrated under reduced pressure to obtain 113.2 g (0.93 mol) of oily 2-chloro-N, N-dimethylacetamide. The yield was 93.1%.
2-Chloro-N,N-dimethylacetamide

506-59-2
79-04-9
2675-89-0
Synthesis of 2-Chloro-N,N-dimethylacetamide from Dimethylamine hydrochloride and Chloroacetyl chloride
Global( 279)Suppliers
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Shaoxing Fangxiao Chemical Co., LTD
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View Lastest Price from 2-Chloro-N,N-dimethylacetamide manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
2-Chloro-N,N-dimethylacetamide pictures 2024-11-26 2-Chloro-N,N-dimethylacetamide
2675-89-0
 US $0.00-0.00 / KG 1KG 99% 20 mt Hebei Weibang Biotechnology Co., Ltd
2-Chloro-N,N-dimethylacetamide pictures 2022-10-18 2-Chloro-N,N-dimethylacetamide
2675-89-0
 US $0.00-0.00 / kg 1kg 98% 1Ton Henan Aochuang Chemical Co.,Ltd.
N,N-Dimethyl-2-chloroacetamide pictures 2021-07-13 N,N-Dimethyl-2-chloroacetamide
2675-89-0
 US $15.00-10.00 / KG 1KG 99%+ HPLC Monthly supply of 1 ton Zhuozhou Wenxi import and Export Co., Ltd
N,N-DIMETHYL-2-CHLOROACETAMIDE N,N-DIMETHYLCHLOROACETAMIDE N,N-DIMETHYLCHOROACETAMIDE CHLOROACETYLDIMETHYLAMINE AKOS BBS-00000943 2-CHLORO-N,N-DIMETHYLACETAMIDE 2-chloro-N,N-dimethyl-ethanamide 2-Chloro-N,N-dimethylacetacetamide 2-Chloro-N,N-dimethy 2-Chloro-N,N-Dimethyl Butylamine 2-CHLORO-N,N-DIMETHYL ACETAMINE Acetamide, 2-chloro-N,N-dimethyl- 2-CHLORO-N N-DIMETHYLACETAMIDE 98 % N-DiMethyl-2-chloroacetaMide 2-chloro -N,N- two MethylacetaMide 2-Chloro-N,N-dimethylacetamide >=97.0% (GC) EOS-61825 2675-89-0 C4H8ClNO 2-Chloro-N,N-dimethylacetamide 2-Chloro-N,N-dimethylacetamide, 97%, 2675-89-0 ClCH2CONCH32 Carbonyl Compounds Building Blocks Amides Organic Building Blocks 2675-89-0