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ChemicalBook--->CAS DataBase List--->98623-50-8

98623-50-8

98623-50-8 Structure

98623-50-8 Structure
IdentificationBack Directory
[Name]

N-Methyl-1H-Indole-5-EthaneSulphonamide
[CAS]

98623-50-8
[Synonyms]

N-Methyl-1H-Indole-5-EthaneSulphomide
N-Methyl-1H-indole-5-ethanesulfonamide
N-Methyl-1H-Indole-5-EthaneSulphonamide
1H-Indole-5-ethanesulfonamide, N-methyl-
2-(1H-indol-5-yl)-N-MethylethanesulfonaMide
N-Methyl-1H-indole-5-ethanesulfonamide, >=98%
2-(1H-indol-5-yl)-N-methylethane-1-sulfonamide
2 - (1h-indole-5-yl) - n-methylethyl-1-sulfonamide
[EINECS(EC#)]

1592732-453-0
[Molecular Formula]

C11H14N2O2S
[MOL File]

98623-50-8.mol
[Molecular Weight]

238.31
Chemical PropertiesBack Directory
[Melting point ]

124-125°C
[Boiling point ]

458.4±47.0 °C(Predicted)
[density ]

1.316±0.06 g/cm3(Predicted)
[storage temp. ]

Keep in dark place,Sealed in dry,Room Temperature
[solubility ]

DMSO (Slightly), Methanol (Slightly)
[form ]

Solid
[pka]

11.52±0.40(Predicted)
[color ]

White to Off-White
Safety DataBack Directory
[Symbol(GHS) ]


GHS07
[Signal word ]

Warning
[Hazard statements ]

H302-H317
[Precautionary statements ]

P280-P305+P351+P338
Hazard InformationBack Directory
[Uses]

N-Methyl-1H-indole-5-ethanesulfonamide is used as a reagent in the synthesis of Naratriptan Hydrochloride (N378730); a triptan drug used for the treatment of migraine headaches.
[General Description]

N-Methyl-1H-Indole-5-EthaneSulphonamide, also known as 2-(1H-Indol-5-yl)-N-methylethanesulfonamide, is a white solid.
[Synthesis]

At 40-45 ℃ (hydrogen pressure: 3-4 kg/cm2), 2-(3-Phenylsulf-anyl-1H-indol-5-yl)-ethanesulfonic acidmethylamide (14) (5 g, 0.014 mol) was hydrogenated in ethanol: water (7:3) (40 ml) in an autoclave for 10 h. After that, the reaction mass was cooled to room temperature, followed by removing the catalyst through filtering. The filtrate was distilled out to get N-Methyl-1H-Indole-5-EthaneSulphonamide. N-Methyl-1H-Indole-5-EthaneSulphonamide
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